A kind of nano-carbon material supporting cobalt-zinc bimetal, its preparation method and application in catalytic oxidation of magnesium sulfite
A nano-carbon material and bimetallic technology, applied in the direction of magnesium sulfate, metal/metal oxide/metal hydroxide catalyst, separation method, etc., can solve the limitation of magnesium sulfate purification and commercial resource application, the influence of magnesium sulfate purity, Environmental pollution and other problems, to achieve the effect of improving the catalytic reaction rate, green process, and strengthening the mass transfer process
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Embodiment 1
[0035] A kind of supported cobalt-zinc bimetallic nano-carbon material of the present embodiment, the preparation method thereof comprises the following steps:
[0036] 1) Synthesis of ZIF-8: Dissolve 5.95 g of zinc acetate hexahydrate in 150 mL of methanol to form a clear solution a; dissolve 6.16 g of 2-methylimidazole in 150 mL of methanol to form a clear solution b. Then slowly add solution b to solution a; stir at 25°C for 24 hours and centrifuge to obtain a white precipitate; then wash with methanol and then dry at 60°C to obtain ZIF-8.
[0037] 2) Preparation of composite carbon material: Disperse the above 0.5g ZIF-8 in 50mL methanol solution to form solution I; dissolve 5.82g cobalt nitrate hexahydrate in 50mL methanol to form solution II; dissolve 6.16g 2-methylimidazole Dissolve in 50 mL methanol to form clear solution III. Then, solution II was slowly added to solution I to form mixed solution IV; then solution III was added to mixed solution IV to form mixed solu...
Embodiment 2
[0040] A kind of supported cobalt-zinc bimetallic nano-carbon material of the present embodiment, the preparation method thereof comprises the following steps:
[0041] 1) Synthesis of ZIF-8: Dissolve 5.95 g of zinc acetate hexahydrate in 150 mL of methanol to form a clear solution a; dissolve 6.57 g of 2-methylimidazole in 150 mL of methanol to form a clear solution b. Then slowly add solution b to solution a; stir at 25°C for 24 hours and centrifuge to obtain a white precipitate; then wash with methanol and then dry at 60°C to obtain ZIF-8.
[0042]2) Preparation of composite carbon material: above-mentioned 0.5g ZIF-8 was dispersed in 50mL methanol solution to form solution I; 11.64g cobalt nitrate hexahydrate was dissolved in 50mL methanol to form solution II; 6.16g 2-methylimidazole Dissolve in 50 mL methanol to form clear solution III. Then, solution II was slowly added to solution I to form mixed solution IV; then solution III was added to mixed solution IV to form mix...
Embodiment 3
[0045] A kind of supported cobalt-zinc bimetallic nano-carbon material of the present embodiment, the preparation method thereof comprises the following steps:
[0046] 1) Synthesis of ZIF-8: Dissolve 5.95 g of zinc acetate hexahydrate in 150 mL of methanol to form a clear solution a; dissolve 6.57 g of 2-methylimidazole in 150 mL of methanol to form a clear solution b. Then slowly add solution b to solution a; stir at 30°C for 30 hours and centrifuge to obtain white precipitate; then wash with methanol and then dry at 60°C to obtain ZIF-8.
[0047] 2) Preparation of composite carbon material: Disperse the above 0.5g ZIF-8 in 50mL methanol solution to form solution I; dissolve 5.82g cobalt nitrate hexahydrate in 50mL methanol to form solution II; dissolve 6.16g 2-methylimidazole Dissolve in 50 mL methanol to form clear solution III. Then, solution II was slowly added to solution I to form mixed solution IV; then solution III was added to mixed solution IV to form mixed soluti...
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