A kind of multifunctional oxidation-resistant magnetic nanocomposite material and preparation method thereof
A nanocomposite material and magnetic nanotechnology, applied in the field of nanobiomedical materials, can solve the problems of difficult to achieve precise targeted delivery and low utilization rate, and achieve precise targeted delivery, good biocompatibility, and excellent anti-oxidation The effect of sex and magnetism
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Embodiment 1
[0029] Weigh 0.7g (35mg / mL) of ferric chloride hexahydrate, 100mg (5mg / mL) of lignin, and 1.8g (90mg / mL) of sodium acetate and dissolve them in 20mL of ethylene glycol, and seal the resulting mixed solution in a 50mL reaction vessel , reacted at 200°C for 10 h, and washed thoroughly with N,N-dimethylformamide and distilled water to obtain a nanocomposite material.
[0030] figure 1 , figure 2 They are the TEM image, the hydrated particle size and the surface potential test image of the nanocomposite material prepared in this example, respectively. Depend on figure 1 , figure 2 It can be seen that the prepared nanocomposite material presents the morphology of nanoclusters, the hydrated particle size is about 304nm, and the surface potential is about -20mV.
[0031] image 3 Test charts of the free radical scavenging rate of the nanocomposite prepared in this example at different concentrations. Depend on image 3 It can be seen that with the increase of concentration, ...
Embodiment 2
[0035]Weigh 0.2g (10mg / mL) of ferric chloride hexahydrate, 200mg (10mg / mL) of lignin, and 1g (50mg / mL) of sodium acetate and dissolve them in 20mL of ethylene glycol, and seal the resulting mixed solution in a 50mL reaction kettle , react at 180°C for 8h, and get the nanocomposite material after fully washing with N,N-dimethylformamide and distilled water.
Embodiment 3
[0037] Weigh 0.4g (20mg / mL) of ferric chloride hexahydrate, 300mg (15mg / mL) of lignin, and 1.4g (70mg / mL) of sodium acetate dissolved in 20mL of ethylene glycol, and seal the resulting mixed solution in a 50mL reaction vessel , reacted at 190°C for 9 hours, and washed thoroughly with N,N-dimethylformamide and distilled water to obtain a nanocomposite material. After testing, the SAR value of the nanocomposite material is 879W / g.
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