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A method for stirring positive electrode slurry

A technology of positive electrode slurry and positive electrode active material, which is applied in chemical instruments and methods, electrode manufacturing, battery electrodes, etc., can solve the problems of sedimentation and positive electrode active material sedimentation, and achieve the effect of avoiding sedimentation

Active Publication Date: 2022-04-22
SUZHOU QINGTAO NEW ENERGY TECH CO LTD
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  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

[0007] Aiming at the problem in the prior art that the density of positive electrode active materials is relatively high, while the density of conductive agents of carbon materials such as graphite is relatively low, in the actual industrial production process, it is very easy to cause sedimentation. The purpose of the present invention is to provide a positive electrode slurry Material stirring method, the method can avoid the use of maleimide-barbituric acid to solve the problem of positive electrode active material sedimentation

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  • A method for stirring positive electrode slurry

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Embodiment 1

[0040] A method for stirring positive electrode slurry:

[0041] The positive electrode slurry (the positive electrode slurry is made up of N-methylpyrrolidone, NCM532 and graphite, and the mass ratio of NCM532 and graphite is 9:1) is added respectively in 5 reaction chambers and carried out stirring process, each reaction The volume of the chamber is 30L; among the 5 reaction chambers, the liquid that is above the height of h1 (the height of h1 accounts for 15% of the total liquid level) circulates in each reaction chamber (the first The liquid whose height from the reaction chamber to the upper liquid level is more than h1 is transferred to the second reaction chamber, and the liquid whose height from the second reaction chamber to the upper liquid level is more than h1 is transferred to the third reaction chamber, and the distance from the third reaction chamber is The liquid whose upper liquid level height is above h1 is transferred to the fourth reaction chamber, and the ...

Embodiment 2

[0045] A method for stirring positive electrode slurry:

[0046] The positive electrode slurry (the positive electrode slurry is composed of N-methylpyrrolidone, NCM811 and Super-P, and the mass ratio of NCM811 and Super-P is 8:1) is added to 10 reaction chambers for stirring process , the volume of each reaction chamber is 50L; In the 10 reaction chambers, the liquid that is above the height of h2 (the height of h2 accounts for 20% of the total liquid level) circulates in each reaction chamber Circulation (the liquid whose height from the first reaction chamber to the upper liquid level is more than h2 is transferred to the second reaction chamber, and the liquid whose height from the second reaction chamber to the upper liquid level is more than h2 is transferred to the third reaction chamber, ... , the tenth reaction chamber is separated from the upper liquid level by h2 and the liquid above is transferred to the first reaction chamber); the stirring process uses two stirri...

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Abstract

The invention relates to a method for stirring positive electrode slurry. The positive electrode slurry includes a solvent, a positive electrode active material, and a conductor; the density of the positive electrode active material is greater than the density of the conductor; the method includes: adding the positive electrode slurry to n reaction chambers for stirring process, the Said n≥2; in said n reaction chambers, the liquid above the liquid level above h circulates in each reaction chamber, and said h accounts for ≥3% of the total liquid level height; said each The actual use volume of the reaction chamber is <300L. In the present invention, through the selection of the reaction chamber, the control of the stirring process (speed and stirring blades), and the circulation setting, the present invention can effectively prevent small-density suspended matter such as graphite from floating on the liquid surface, and avoid the gap between each parallel stirring chamber. There is a concentration difference between them, and then the effect of avoiding the use of maleimide-barbituric acid to solve the sedimentation of the positive electrode active material can be achieved.

Description

technical field [0001] The invention belongs to the technical field of battery preparation, and in particular relates to a method for stirring positive electrode slurry. Background technique [0002] The existing positive electrode materials are mainly composed of positive electrode active materials, conductive agents, lithium salts and binders, and most of the positive electrode active materials are layered metal oxides with a certain crystal structure (such as LiCoO 2 etc.), the conductive agent is usually carbon materials such as graphite, carbon black, carbon fiber, etc., and the binder mainly plays a role in bonding between the active material layers, and is used for bonding between the active material layer and the current collector. , the density of the positive electrode active material is much higher than that of the conductive agent and the binder, and with the increasing demand for energy density and the use of ternary materials, this density difference tends to g...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): B01J19/18B01J19/00B01F33/80H01M4/04H01M4/36
CPCB01J19/18B01J19/0006H01M4/04H01M4/36B01F33/812B01F33/81B01F33/813Y02E60/10
Inventor 李峥冯玉川何泓材周柯王丹丹杨帆南策文
Owner SUZHOU QINGTAO NEW ENERGY TECH CO LTD
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