Preparation method of flower-like nano-palladium/foamed nickel catalytic material and application of flower-like nano-palladium/foamed nickel catalytic material in electrocatalytic reduction dechlorination reaction
A catalytic material and nickel foam technology, which are applied in catalyst activation/preparation, chemical instruments and methods, physical/chemical process catalysts, etc., can solve the problems of high dechlorination efficiency, long dechlorination time, and complex catalytic material preparation technology. , to achieve the effects of high dechlorination efficiency, low cost and simple preparation method
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Embodiment 1
[0031] First put the nickel foam (2cm*2cm*1.2cm) electrode into acetone for ultrasonic degreasing, then soak it in 0.5mol / L dilute sulfuric acid to remove surface oxides, then clean it with ultrasonic oscillation in distilled water, and finally use high Dry it with pure nitrogen and save it for later use.
[0032] Get a piece of cleaned foam nickel (2cm*2cm*1.2cm) and put it into 40ml of 0.25mmol / L palladium chloride solution (the concentration of palladium chloride in the mixed solution), the amount of palladium chloride and sodium chloride The ratio is 1:500, react in a shaker at 25°C with a speed of 160 times / min for 0.5h, the light yellow color of the solution recedes, take out the electrode and rinse it gently with deionized water for 3 times, dry it with nitrogen, and prepare a flower The nanometer palladium / foam nickel catalytic electrode is used as the working electrode. The dechlorination reaction is an H-type three-electrode system: the prepared flower-shaped nano-p...
Embodiment 2
[0034] First put the nickel foam (2cm*2cm*1.2cm) electrode into acetone for ultrasonic degreasing, then soak it in 0.5mol / L dilute sulfuric acid to remove surface oxides, then clean it with ultrasonic oscillation in distilled water, and finally use high Dry it with pure nitrogen and save it for later use.
[0035]Take a piece of cleaned foam nickel (2cm*2cm*1.2cm) and put it into 40ml of 0.5mmol / L palladium chloride solution (the concentration of palladium chloride in the mixed solution), the amount of palladium chloride and sodium chloride The ratio is 1:100, react in a shaker at 40°C with a speed of 160 times / min for 2 hours, the light yellow color of the solution fades, take out the electrode and rinse it gently with deionized water for 3 times, dry it with nitrogen, and prepare a flower shape The nano-palladium / nickel foam catalytic electrode is used as the working electrode. The dechlorination reaction is an H-type three-electrode system: the prepared flower-shaped nano-...
Embodiment 3
[0037] First put the nickel foam (2cm*2cm*1.2cm) electrode into acetone for ultrasonic degreasing, then soak it in 0.5mol / L dilute sulfuric acid to remove surface oxides, then clean it with ultrasonic oscillation in distilled water, and finally use high Dry it with pure nitrogen and save it for later use.
[0038] Get a piece of cleaned foam nickel (2cm*2cm*1.2cm) and put it into 40ml 2mmol / L palladium chloride solution (the concentration of palladium chloride in the mixed solution), the ratio of the amount of palladium chloride and sodium chloride 1:100, reacted at 30°C for 2 hours in a shaker with a speed of 160 times / min, the light yellow color of the solution receded, took out the electrode and rinsed it gently with deionized water for 3 times, and dried it with nitrogen to prepare a flower-shaped nanometer The palladium / nickel foam catalytic electrode is used as the working electrode. The dechlorination reaction is an H-type three-electrode system: the prepared flower-sh...
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