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A regulation (feconicralcu) p /2024A1 Methods of Composites Interfaces

A composite material and interface technology, which is applied in the heat treatment of interface regulation and regulation of the heat treatment field of p/2024A1 composite material interface, can solve the problem that the potential of strength and toughness cannot be fully exerted, the interface features are lacking, and the bonding strength and thickness of the composite material interface are ideal. Status and other issues

Active Publication Date: 2021-09-10
JIANGSU UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, at present, most scientific researchers adopt measures to improve the strength and toughness by optimizing the types and properties of strengthening particles, and the control of interface characteristics is relatively lacking, which cannot make the bonding strength and thickness of the interface of composite materials reach the ideal state, which often leads to the strengthening of high-entropy alloys. The potential of strength and toughness of aluminum matrix composites cannot be fully realized

Method used

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  • A regulation (feconicralcu)  <sub>p</sub> /2024A1 Methods of Composites Interfaces
  • A regulation (feconicralcu)  <sub>p</sub> /2024A1 Methods of Composites Interfaces

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Effect test

Embodiment 1

[0029] (FeCoNiCrAlCu) provided by the present invention p / 2024A1 A method for regulating the interface structure of composite materials, including the following steps:

[0030] Iron powder, cobalt powder, nickel powder, chromium powder, aluminum powder, copper powder and other powders with a purity of 99.9% are mixed according to an equiatomic ratio, placed in a ball mill tank, vacuumed and argon gas is introduced, and then high-energy High-entropy alloy powders were prepared by ball milling and mechanical alloying. Mix the high-entropy alloy powder and 2024Al powder according to the addition amount of the reinforcing phase at 10wt.%, to obtain a composite material powder, and then carry out cold isostatic pressing at a pressure of 250 MPa for 2 minutes, and the block after cold isostatic pressing Perform microwave sintering at 480°C for 40 minutes to make (FeCoNiCrAlCu) with interface regulation and heat treatment p / 2024A1 composite material base material

[0031] First,...

Embodiment 2

[0035] Iron powder, cobalt powder, nickel powder, chromium powder, aluminum powder, copper powder and other powders with a purity of 99.9% are mixed according to an equiatomic ratio, placed in a ball mill tank, vacuumed and argon gas is introduced, and then high-energy High-entropy alloy powders were prepared by ball milling and mechanical alloying. Mix the high-entropy alloy powder and 2024Al powder according to the addition amount of the reinforcing phase at 15wt.%, to obtain a composite material powder, and then carry out cold isostatic pressing at a pressure of 250 MPa for 2 minutes, and the block after cold isostatic pressing Perform microwave sintering at 480°C for 40 minutes to produce (FeCoNiCrAlCu) p / 2024A1 composite base material.

[0036] First, the prepared (FeCoNiCrAlCu) p / 2024A1 Composite material base material is placed in WBMW-X4 microwave sintering furnace for solid solution treatment. Vacuumize the furnace and fill it with nitrogen, heat at 45°C / min to 30...

Embodiment 3

[0040] Iron powder, cobalt powder, nickel powder, chromium powder, aluminum powder, copper powder and other powders with a purity of 99.9% are mixed according to an equiatomic ratio, placed in a ball mill tank, vacuumed and argon gas is introduced, and then high-energy High-entropy alloy powders were prepared by ball milling and mechanical alloying. Mix the high-entropy alloy powder and 2024Al powder according to the addition amount of the reinforcing phase at 20wt.%, to obtain a composite material powder, and then perform cold isostatic pressing at a pressure of 250 MPa for 2 minutes, and the block after cold isostatic pressing Perform microwave sintering at 480°C for 40 minutes to produce (FeCoNiCrAlCu) p / 2024A1 Composite material parent material;

[0041] The prepared (FeCoNiCrAlCu) p / 2024A1 Composite material base material is put into WBMW-X4 microwave sintering furnace, vacuumize the furnace and fill it with nitrogen, heat at 50°C / min to 300°C for 4 minutes, then rapi...

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Abstract

The present invention provides a control (FeCoNiCrAlCu) p / 2024A1 The method of composite material interface belongs to the technical field of metallurgy and heat treatment of metal materials. The present invention will (FeCoNiCrAlCu) p / 2024A1 Composite block base material is placed in a microwave sintering furnace, and the microwave sintering process is used for solution treatment and aging treatment. Through heat treatment, the material interface diffusion is promoted, and the interface characteristics are adjusted, thereby adjusting the thickness of the diffusion layer and the interface mechanical properties, and improving Strength and toughness of composite materials.

Description

technical field [0001] The invention belongs to the technical field of metallurgy and heat treatment of metal materials, and relates to a heat treatment method for interface control of high-entropy alloy particle reinforced aluminum-based composite materials, especially for control (FeCoNiCrAlCu) p / 2024A1 Heat treatment method for composite interface. Background technique [0002] High-entropy alloy is a brand-new alloy system with unique microstructure, high hardness and strength, and good thermal stability at high temperature. And because of the natural interfacial bonding characteristics between metal and metal, the interfacial wettability and interfacial compatibility between the high-entropy alloy and the aluminum alloy matrix are good. If the high-entropy alloy is used as the composite phase to strengthen the aluminum alloy, and through the interface The control of the characteristics will realize the simultaneous improvement of the strength and plasticity of the com...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C22F1/02C22F1/04B22F3/105B22F9/04B22F3/24
CPCB22F3/105B22F3/24B22F9/04B22F2003/1054B22F2003/248B22F2009/041B22F2009/043B22F2998/10C22F1/002C22F1/02C22F1/04B22F1/0003B22F3/04
Inventor 高立鹏李桂荣王宏明任文祥文浩然
Owner JIANGSU UNIV