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Method for detecting reinforcing property of carbon black in natural rubber based on binding glue

A technology of natural rubber and binding rubber, applied in measuring devices, mechanical thickness measurement, instruments, etc., can solve the problems of unreported carbon black reinforcement performance, research can not be widely carried out, and measurement methods cannot be found, and achieve good application prospects. , The detection picture is clear and the effect of ensuring the accuracy

Active Publication Date: 2020-11-06
SICHUAN UNIVERSITY OF SCIENCE AND ENGINEERING
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

At present, by soaking the mixed rubber in a benign solvent and measuring the weight loss of the tested rubber sample to calculate the binding rubber content, the operation is cumbersome
However, due to the fact that there is no suitable measurement method for the performance of the binder, the research in this area cannot be widely carried out, and there is no report about the reinforcement performance of carbon black by measuring the thickness of the binder.

Method used

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  • Method for detecting reinforcing property of carbon black in natural rubber based on binding glue
  • Method for detecting reinforcing property of carbon black in natural rubber based on binding glue
  • Method for detecting reinforcing property of carbon black in natural rubber based on binding glue

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0030] 1) The rubber compound formula consists of the following components in mass parts: 100 parts of natural rubber, 50 parts of N115 carbon black, 3 parts of stearic acid, 5 parts of zinc oxide, 0.6 parts of accelerator DM, and 1.5 parts of sulfur. After weighing the ingredients according to the formula, the mixing process is carried out according to the national standard. The specific experimental steps are as follows:

[0031] S1: Dry the carbon black raw material in a drying oven before mixing, and place it in a clean environment after drying.

[0032] S2: During mixing, firstly, the operating distance between the two baffles is 200 mm, and the roller temperature is controlled at 70 °C. The rubber is wrapped on the front roller, and the knife is cut twice for 2 minutes. Then adjust the roller distance to 1.65 mm, add stearic acid, cut the knife once during the period, and operate for 2.5 minutes. Add the mixture of sulfur, vulcanization accelerator and zinc oxide, and ...

Embodiment 2

[0040] 1) The compounding formula consists of the following components by mass: 100 parts of natural rubber, 50 parts of N330 carbon black, 3 parts of stearic acid, 5 parts of zinc oxide, 0.6 parts of accelerator DM, and 1.5 parts of sulfur. After weighing the ingredients according to the formula, the mixing process is carried out according to the national standard. The specific experimental steps are as follows:

[0041] S1: Dry the carbon black raw material in a drying oven before mixing, and place it in a clean environment after drying.

[0042] S2: During mixing, firstly, the operating distance between the two baffles is 200 mm, and the roller temperature is controlled at 70 °C. The rubber is wrapped on the front roller, and the knife is cut twice for 2 minutes. Then adjust the roller distance to 1.65 mm, add stearic acid, cut the knife once during the period, and operate for 2.5 minutes. Add the mixture of sulfur, vulcanization accelerator and zinc oxide, and add in two...

Embodiment 3

[0049] 1) The compounding formula consists of the following components in mass parts: 100 parts of natural rubber, 50 parts of N550 carbon black, 3 parts of stearic acid, 5 parts of zinc oxide, 0.6 parts of accelerator DM, and 1.5 parts of sulfur. After weighing the ingredients according to the formula, the mixing process is carried out according to the national standard. The specific experimental steps are as follows:

[0050] S1: Dry the carbon black raw material in a drying oven before mixing, and place it in a clean environment after drying.

[0051] S2: During mixing, firstly, the operating distance between the two baffles is 200 mm, and the roller temperature is controlled at 70 °C. The rubber is wrapped on the front roller, and the knife is cut twice for 2 minutes. Then adjust the roller distance to 1.65 mm, add stearic acid, cut the knife once during the period, and operate for 2.5 minutes. Add the mixture of sulfur, vulcanization accelerator and zinc oxide, and add ...

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Abstract

The invention discloses a method for detecting the reinforcing property of carbon black in natural rubber based on binding glue. After sampling by an ultra-thin freezing slicing machine, when a tapping mode of an atomic force microscope is used for characterizing the carbon black-rubber composite material, the characteristics of the binding glue of the carbon black reinforced composite material can be directly observed by utilizing the difference between the imaging characteristics of a topography diagram and a phase diagram, so that the thickness of the binding glue is obtained, and the influence of the binding glue on the rubber performance and the reinforcing performance of carbon black in rubber are analyzed. The method has the advantages of simple operation, no need of excessive treatment on the sample, high detection efficiency, clear detection picture, high detection accuracy and the like, has better applicability, and provides a new method and thought for researching the reinforcement of filler.

Description

technical field [0001] The invention belongs to the technical field of rubber composite materials, and in particular relates to a method for detecting the reinforcing performance of carbon black in natural rubber based on binding glue. Background technique [0002] After more than 130 years of development, the automobile industry is now an important force to promote a new round of technological revolution and industrial revolution, an important support for building a powerful country, and an important pillar of the national economy. It is closely related to the travel of the people and the improvement of ecological civilization. Car tires are an important component of the car, which play the role of bearing the full weight of the car and ensuring good adhesion between the wheel and the road. The tire tread is the part that is in direct contact with the ground. The quality of the tread rubber directly affects the safety and ride comfort of the car. Therefore, as a reinforcing...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): G01Q60/24
CPCG01Q60/24G01Q30/20G01Q60/34C08K3/04C08L7/00C08K3/30C08K5/36C08K13/02C08K2003/2296C08K2201/014G01B5/06
Inventor 陈建雷智强唐成玉刘莎何宇李瑞卿龙刘平李琳龚勇
Owner SICHUAN UNIVERSITY OF SCIENCE AND ENGINEERING