Transparent flexible nano composite base material as well as preparation method and application thereof
A nano-composite and transparent technology, applied in chemical instruments and methods, synthetic resin layered products, lamination, etc., can solve the problems of prone to yellowing and poor long-term use effect, and achieve control of yellowing, high The effect of transmittance
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Synthetic example 1
[0026] 1. Add all monomers acrylic acid, n-butyl acrylate, acrylonitrile, initiator benzoyl peroxide, and butyl into a 500ml four-necked flask, and stir to form an emulsion.
[0027] 2. Transfer 2 / 3 of the emulsion to a constant pressure dropping funnel for titration.
[0028] 3. The temperature of the water bath is raised to 82°C, and the reaction is slowly added dropwise with a constant pressure dropping funnel, and the temperature is kept at 82±2.0°C to prevent the reaction from being violent; the dropwise addition is completed in 3 hours.
[0029] 4. Turn off the heating after dripping, stir and cool down to normal temperature, and the synthesis is completed.
[0030] The specific addition amount is shown in Table 1 below:
[0031] Table 1
[0032] acrylic acid 4.0g n-butyl acrylate 35.0g Acrylonitrile 10.00g Benzoyl peroxide 0.02g Butyl ester 50.98g total 100.00g
[0033] 5. In the synthesized acrylic resin, add 10 parts of t...
Synthetic example 2
[0035] Complete according to steps 1-4 of Synthesis Example 1, and the specific addition amount is shown in Table 2 below.
[0036] Table 2
[0037] acrylic acid 3.00g n-butyl acrylate 35g Acrylonitrile 11.00g Benzoyl peroxide 0.02g Butyl ester 50.98g total 100.00g
[0038] 5. In the synthesized acrylic resin, add 10 parts of transparent nano powder for every 100 parts.
Embodiment 1
[0047] Coat the adhesive of Synthesis Example 1 on the optical PET with a thickness of 20 microns, and at a maximum pressing temperature of 80°C, laminate a 35-micron VLP copper foil, bake and cure in an oven, and the maximum curing temperature is 160°C.
[0048] The main characteristics of the finished product are shown in Table 4
[0049] Table 4
[0050]
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