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Water pollution analysis method based on ultraviolet visible spectrum and three-dimensional fluorescence spectrum

A three-dimensional fluorescence and analysis method technology, applied in the field of water pollution analysis, can solve the problems of low analysis efficiency, scattering, inaccurate quantitative detection results, etc., and achieve the effect of small relative error, guaranteed accuracy, and data simplification

Pending Publication Date: 2020-11-24
安徽思环科技有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004] With the development of industry, the components contained in sewage are complex, such as non-corroded fat and other biological macromolecules with uneven particle size distribution, which will produce scattering when irradiated by ultraviolet rays, resulting in inaccurate quantitative detection results, which makes it difficult to ensure the realization of the components in polluted water. Accurate analysis, and a large amount of analysis data, the analysis efficiency of existing devices is low, and cannot meet people's use requirements, so it is necessary to study a water pollution analysis method based on ultraviolet-visible spectroscopy and three-dimensional fluorescence spectroscopy

Method used

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  • Water pollution analysis method based on ultraviolet visible spectrum and three-dimensional fluorescence spectrum
  • Water pollution analysis method based on ultraviolet visible spectrum and three-dimensional fluorescence spectrum

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Embodiment 1

[0032] see figure 1 and 2 , in the embodiment of the present invention, a water pollution analysis method based on ultraviolet visible spectrum and three-dimensional fluorescence spectrum, the specific steps of the operation method are:

[0033] Step 1: Sampling of water quality, through sampling equipment to conduct multi-point sampling of the water source for analysis, and then make polluted water samples and pure water samples.

[0034] Step 2: Collect the three-dimensional fluorescence spectrum, and irradiate the water samples collected in multiple bottles, polluted water samples and pure water samples with ultraviolet rays to reflect fluorescence signals, and the fluorescence signals generate three-dimensional fluorescence spectra through the diffraction grating.

[0035] Step 3: conversion of the three-dimensional fluorescence spectrum. The three-dimensional fluorescence spectrum is converted into an electrical signal through a CMOS chip, thereby obtaining three-dimensi...

Embodiment 2

[0040] see figure 2 , in the embodiment of the present invention, the sampling of water quality comprises sampling device, and sampling device comprises unmanned aerial vehicle body, fixing frame, collection dish, extracting mechanism and control mechanism, and fixing frame is rotatably installed on the lower end position of drone body, and collecting dish There are multiple sets and they are evenly fixed on the fixed frame. The input end of the extraction mechanism is set on the lower side of the collection dish, and the output end of the extraction machine is placed on the input end of the collection dish. The control mechanism is installed on the drone body.

[0041] The sampling device also includes a backwashing mechanism, and the backwashing mechanism is arranged on the output end of the extraction mechanism, and the input and output ends of the extraction mechanism are fixed with control valves, so that the extraction mechanism can be washed with water after a single sa...

Embodiment 3

[0044] see figure 1 , in the embodiment of the present invention, the ultraviolet light in the three-dimensional fluorescence spectrum is collected by outputting monochromatic ultraviolet light through the laser array, the excitation wavelength of the monochromatic ultraviolet light is 300-500nm, and the emission wavelength is 450-650nm, so that the ultraviolet light is irradiated to generate The spectrum is more significant, which provides a certain guarantee for the extraction of subsequent spectral data.

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Abstract

The invention discloses a water pollution analysis method based on an ultraviolet visible spectrum and a three-dimensional fluorescence spectrum. The specific steps of the operation method are as follows: sampling water quality, namely carrying out multi-point sampling on an analysis water source through sampling equipment, and then preparing a polluted water sample and a purified water sample; collecting a three-dimensional fluorescence spectrum, namely irradiating multiple bottles of collected water samples, polluted water samples and purified water samples through ultraviolet rays to reflect fluorescence signals, and enabling the fluorescence signals to generate the three-dimensional fluorescence spectrum through a diffraction grating; converting a three-dimensional fluorescence spectrum, namely converting the three-dimensional fluorescence spectrum into an electric signal through a CMOS chip so as to obtain three-dimensional fluorescence spectrum data in the form of the electric signal; processing the three-dimensional fluorescence spectrum data, namely preprocessing the three-dimensional fluorescence spectrum data. The method is reasonable in design and accurate in analysis, the three-dimensional fluorescence spectrum data can be corrected, the accuracy of sewage analysis data is well guaranteed, and a certain scientific basis is provided for a water pollution treatment method.

Description

technical field [0001] The invention belongs to the technical field of water pollution analysis methods, in particular to a water pollution analysis method based on ultraviolet visible spectrum and three-dimensional fluorescence spectrum. Background technique [0002] Water pollution is the reduction or loss of the use value of water caused by harmful chemical substances, polluted water, acids, alkalis, oxidants in sewage, and compounds such as copper, cadmium, mercury, arsenic, benzene, dichloroethane, ethylene dichloride, etc. Alcohol and other organic poisons will kill aquatic organisms and affect drinking water sources and scenic spots. When organic matter in sewage is decomposed by microorganisms, it will consume oxygen in water and affect the life of aquatic organisms. After the dissolved oxygen in water is exhausted, organic matter will be anaerobic. Decomposition produces unpleasant gases such as hydrogen sulfide and mercaptans, further deteriorating water quality, s...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): G01N21/64G01N21/31
CPCG01N21/64G01N21/31G01N2021/6419
Inventor 丁训林杨齐红王万青孙刚忠李明超任福林
Owner 安徽思环科技有限公司
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