A kind of rapidly disintegrating sulfur granule composition and preparation method thereof
A technology of sulfur granules and compositions, applied in fertilizer mixtures, applications, potash fertilizers, etc., can solve the problems of complex control process routes, difficulty in large-scale mass production, and high preparation costs, and achieve excellent dispersion stability, easy packaging, and improved The effect of crop quality
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Embodiment 1
[0027] ① Fully mix 150g of magnesium aluminum silicate with 800g of molten liquid sulfur, cool to room temperature, then use a crusher to crush and grind to prepare sulfur / magnesium aluminum silicate fine powder with a particle size of 1100 mesh;
[0028] ② Add the sulfur / magnesium aluminum silicate powder prepared in step ①, 10g calcium lignosulfonate, 20g potassium chloride, 10g xanthan gum and 10g zinc oxide into water and mix them in turn, and mix them with a planetary mill for 40 minutes , to obtain a mixed solution A;
[0029] ③ The mixed solution A obtained in step ② is freeze-dried, and then ground to a mesh number of 200 mesh to obtain the sulfur particle composition B;
[0030] ④ Granulate the sulfur granule composition B prepared in step ③ at 150°C to obtain a rapidly disintegrating sulfur granule composition;
[0031] The prepared sulfur granule composition disintegrates when exposed to water for 60 seconds, and the disintegration fineness D(3,2)>500 mesh.
Embodiment 2
[0033] ① Fully mix 150g of magnesium aluminum silicate with 785g of molten liquid sulfur, cool to room temperature, then use a crusher to crush and grind to prepare sulfur / magnesium aluminum silicate fine powder with a particle size of 1200 mesh;
[0034] ② Add the sulfur / magnesium aluminum silicate powder prepared in step ①, 15g calcium lignosulfonate, 20g potassium chloride, 20g xanthan gum and 10g zinc oxide into water and mix them in turn, and mix them with a planetary mill for 60 minutes , to obtain a mixed solution A;
[0035] ③ The mixed solution A obtained in step ② is freeze-dried, and then ground to a mesh number of 200 mesh to obtain the sulfur particle composition B;
[0036] ④ Granulate the sulfur granule composition B prepared in step ③ at 130°C to obtain a rapidly disintegrating sulfur granule composition;
[0037] The prepared sulfur granule composition disintegrates when exposed to water for 40 seconds, and the disintegration fineness D(3,2)>500 mesh.
Embodiment 3
[0039] ① Fully mix 150g of magnesium aluminum silicate with 780g of molten liquid sulfur, cool to room temperature, then use a crusher to crush and grind to prepare sulfur / magnesium aluminum silicate fine powder with a particle size of 1500 mesh;
[0040] ② Add the sulfur / magnesium aluminum silicate powder prepared in step ①, 20g calcium lignosulfonate, 20g potassium chloride, 20g xanthan gum and 10g zinc oxide into water and mix them in turn, and mix them with a planetary mill for 30 minutes , to obtain a mixed solution A;
[0041] ③ The mixed solution A obtained in step ② is freeze-dried, and then ground to a mesh number of 200 mesh to obtain the sulfur particle composition B;
[0042] ④ Granulate the sulfur granule composition B prepared in step ③ at 140°C to obtain a rapidly disintegrating sulfur granule composition;
[0043] The prepared sulfur granule composition disintegrates when exposed to water for 30 seconds, and the disintegration fineness D(3,2)>500 mesh.
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