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Polarizer preparation method

A technology of polarizers and polarizers, applied in chemical instruments and methods, optics, polarizing elements, etc., can solve the problems of peeling, peeling, and random distribution of bright spots at the bonding interface, and achieve surface compatibility improvement and drying condition optimization , Reduce the effect of crack point defects

Active Publication Date: 2021-01-22
SHENZHEN SAPO PHOTOELECTRIC
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, water-based adhesives sometimes peel off at the bonding interface under humidified conditions
In view of the above problems, the prior art has proposed adhesives for polarizers containing acetoacetyl group-containing polyvinyl alcohol-based resins and cross-linking agents. Although this method introduces hydrophobic groups, it can effectively improve the performance of PVA water-based adhesives in high-humidity environments. However, it also introduces the problem of incompatibility of the bonding interface. There is no obvious improvement in solving the crack point problem, which is manifested as bright spots and bright lines randomly distributed, and even peeling at the bonding interface. , will seriously affect the display effect

Method used

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  • Polarizer preparation method

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0057] Swell a polyvinyl alcohol resin film (PVA film) with a thickness of 75 μm in deionized water at 30° C. for 2 minutes, and dissolve it in an aqueous solution containing 0.08 wt % iodine (which contains KI, and the weight ratio iodine: KI=1:16) , soaked at 30°C for 1 minute to absorb dichroic substances, then washed with pure water for 15 seconds, then soaked in a mixed aqueous solution of 55°C containing 4wt% boric acid and 5wt% KI, and extended to the original Membrane 5.5 times, followed by washing with deionized water for 10 seconds at room temperature, into the plain membrane to dry.

[0058] The plain film drying is divided into four sections, low temperature section: temperature 40 ℃, humidity 80% RH, residence time 45 seconds; medium temperature section: temperature 48 ℃, humidity 80% RH, residence time 100 seconds; high temperature section: temperature 78 ℃, humidity 70 %RH, residence time 30 seconds; cooling section: temperature 40℃, humidity 60%RH, residence ti...

Embodiment 2

[0064] The specific drying process of Example 2-Experimental Example 4, Comparative Example 1-Comparative Example 3 is shown in Table 1, and the sample preparation and testing process are consistent with those of Example 1.

[0065] Table 1 embodiment and the plain film drying condition contrast table of comparative example

[0066]

[0067] Examples and comparative examples were detected according to the detection content and detection method as described in Example 1, and the results are shown in Table 2.

[0068] Table 2 Comparison table of crack point defect inspection results of embodiment and comparative example

[0069] A test B test Degree of polarization (%) Transmittance (%) Moisture content (%) Remark Example 1 1 2 99.97 42.3 2.88 Example 2 0 1 99.92 42.5 2.54 Example 3 1 2 99.93 42.4 2.21 Example 4 2 2 99.94 42.5 2.75 Comparative example 1 18 21 99.93 42.4 2.59 Comparative exam...

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Abstract

The invention provides a polarizer preparation method, which comprises: drying a dyed, stretched and cleaned PVA film at a drying temperature of 40-95 DEG C under a drying environment humidity of 50-100% RH to make the moisture content of the obtained plain film be 2-5 wt%; and forming a protective layer on the surface of the film to obtain the polarizer. By means of the technical scheme, on the premise that an existing polaroid manufacturing process is not changed basically, the drying conditions of the dyed, stretched and cleaned PVA film are optimized, the surface compatibility of the plainfilm is improved, the occurrence rate of cracking point defects and the like is effectively reduced, and therefore the product quality is improved.

Description

technical field [0001] The invention belongs to the technical field of polarizer preparation, and in particular relates to a method for preparing a polarizer. Background technique [0002] With the "ubiquitous" display technology, as a necessary part of the display - polarizer (ie, polarizer) is also increasingly used in the field. But what follows is that the performance requirements of polarizers are becoming more and more stringent in order to adapt to the widely varying use environments. [0003] Polarizers are usually obtained by uniaxially stretching films after dyeing polyvinyl alcohol-based films and dichroic materials (such as iodine, special dyes, etc.). Because it is made by stretching, the polarizer is easy to shrink and deform in harsh environments such as heat and humidity (such as ambient temperature higher than 60°C, humidity environment close to condensation, etc.), which in turn makes its optical properties (such as polarization) Decrease in degree, etc.)...

Claims

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Application Information

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IPC IPC(8): B32B37/12B32B38/00B32B38/14B32B38/16G02B5/30
CPCB32B37/12B32B38/162B32B38/164B32B38/14G02B5/305
Inventor 钟伟宏赵庆飞张卓莉谌臻陈传友范俊彬
Owner SHENZHEN SAPO PHOTOELECTRIC
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