Infrared nonlinear optical crystal KAg3Ga8Se14 as well as preparation method and application thereof
A technology of nonlinear optics and crystals, applied in nonlinear optics, chemical instruments and methods, optics, etc., can solve problems such as limited applications, and achieve stable existence, stable physical and chemical properties, and good repeatability
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[0025] Weigh Ag according to the molar ratio of Ag:Ga:Se =3:8:14 2 O, Ga 2 o 3 and Se, add excess potassium iodide as K source and flux, add Ag 2 O, Ga 2 o 3 The B element in the corresponding molar ratio (B:O = 2:3) of the oxygen element in it is used as the reducing agent. After mixing and grinding, it was pressed into tablets, then sealed in a vacuumized quartz tube with a flame, reacted at 950 °C for more than 24 hours, and then slowly cooled to 300 °C at a cooling rate of 5 °C / hour to obtain orange KAg 3 Ga 8 Se 14 The product of the crystal is washed with distilled water or absolute ethanol, separated by ultrasonic treatment, and dried to obtain KAg 3 Ga 8 Se 14 crystals. Analysis by single crystal X-ray diffraction showed that the compound was KAg 3 Ga 8 Se 14 , the crystal parameters are as follows:
[0026] The unit cell parameters for this compound are: a = 12.8805(5) Å, b = 11.6857(4) Å, c = 9.6600(4) Å, α = gamma = 90°, β = 115.9980(1)°, Z...
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