Preparation method of branched chain amino acid chelated copper
A branched-chain amino acid and chelated copper technology, which is applied in the preparation of organic compounds, chemical instruments and methods, and cyanide reaction preparation, can solve the problems of complex proportioning, difficulty in control, and inconvenience, and achieve high quality and fine process perfect effect
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Embodiment 1
[0027] see Figure 1-2 , a kind of embodiment provided by the invention: a kind of preparation method of branched-chain amino acid chelated copper, the preparation method of described branched-chain amino acid chelated copper comprises the following steps:
[0028] (1) Add raw materials in autoclave;
[0029] (2) the high pressure reaction kettle is heated to obtain the reaction solution;
[0030] (3) the reaction solution is carried out cooling crystallization in the crystallization kettle;
[0031] (4) centrifuging and drying the crystallization solution;
[0032] (5) crush and sieve the dried product, and put it into a sterilization box for sterilization;
[0033] (6) Packaging obtains food-grade branched-chain amino acid copper.
[0034] Specifically, the raw materials in the step (1) include branched chain amino acids, copper source and water.
[0035] Specifically, the branched-chain amino acid is food-grade valine.
[0036] Specifically, the copper source is food-...
Embodiment 2
[0043] see Figure 1-3 , a kind of embodiment provided by the invention: a kind of preparation method of branched-chain amino acid chelated copper, the preparation method of described branched-chain amino acid chelated copper comprises the following steps:
[0044] (1) Add raw materials in autoclave;
[0045] (2) the high pressure reaction kettle is heated to obtain the reaction solution;
[0046] (3) the reaction solution is carried out cooling crystallization in the crystallization kettle;
[0047] (4) centrifuging and drying the crystallization solution;
[0048] (5) crush and sieve the dried product, and put it into a sterilization box for sterilization;
[0049] (6) Packaging obtains food-grade branched-chain amino acid copper.
[0050] Specifically, the raw materials in the step (1) include branched chain amino acids, copper source and water.
[0051] Specifically, the branched-chain amino acid is food-grade leucine.
[0052] Specifically, the copper source is food...
Embodiment 3
[0059] see Figure 1-4 , a kind of embodiment provided by the invention: a kind of preparation method of branched-chain amino acid chelated copper, the preparation method of described branched-chain amino acid chelated copper comprises the following steps:
[0060] (1) Add raw materials in autoclave;
[0061] (2) the high pressure reaction kettle is heated to obtain the reaction solution;
[0062] (3) the reaction solution is carried out cooling crystallization in the crystallization kettle;
[0063] (4) centrifuging and drying the crystallization solution;
[0064] (5) The dried product is crushed and sieved, and put into a sterilization box for sterilization.
[0065] (6) packaging obtains food-grade branched-chain amino acid copper;
[0066] Specifically, the raw materials in the step (1) include branched chain amino acids, copper source and water.
[0067] Specifically, the branched-chain amino acid is food-grade isoleucine.
[0068]Specifically, the copper source is...
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