Temperature-sensitive adhesion type bridging leaking stoppage system, leaking stoppage slurry and preparation method and application of temperature-sensitive adhesion type bridging leaking stoppage system and leaking stoppage slurry
A temperature-sensitive adhesion type, bridging plugging technology, applied in chemical instruments and methods, instruments, drilling compositions, etc., can solve the problems of low success rate of one-time plugging, poor adhesion of crack walls, damage, etc. Achieve the effect of enhancing plugging strength and stability, stable melting temperature and overcoming low strength
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Embodiment 1
[0071] A temperature-sensitive adhesive bridging plugging system, comprising the following raw materials in mass percentage: 40% of temperature-sensitive adhesive resin particles, 25% of rigid particle materials, 25% of elastic particle materials, and 10% of fiber materials;
[0072] Wherein, the rigid particle material is walnut shell particles; the elastic particle material is rubber particles; the fiber material is polyamide fiber;
[0073] The temperature-sensitive adhesive resin particles are prepared according to the following method:
[0074] (1) Preparation of modified solid-phase filled melting range modifiers
[0075] Add 25g of oven-dried silicon dioxide (90nm particle size) into 500mL of dichloromethane, and ultrasonically disperse for 30min to obtain a suspension a; add 20mL of vinyltrimethoxysilane dropwise to the suspension a for a time of 30 minutes, ultrasonic dispersion for 10 minutes to obtain a suspension b, then stand at 70°C for 8 hours, centrifuge, and ...
Embodiment 2
[0088] A temperature-sensitive adhesive bridging plugging system, comprising the following raw materials in mass percentage: 40% of temperature-sensitive adhesive resin particles, 25% of rigid particle materials, 25% of elastic particle materials, and 10% of fiber materials;
[0089] Wherein, the rigid particle material is walnut shell particles; the elastic particle material is rubber particles; the fiber material is polyamide fiber;
[0090] The preparation method of the temperature-sensitive adhesive resin particles is as follows:
[0091] (1) Preparation of modified solid-phase filled melting range regulator:
[0092] Add 25g of dried zeolite powder (with a particle size of 10μm) into 500mL of dichloromethane, and ultrasonically disperse for 30min to obtain suspension a; add 20mL of vinyltrimethoxysilane dropwise to suspension a for 30min , ultrasonically dispersed for 10 minutes to obtain a suspension b, then left to react at 70°C for 8 hours, centrifuged, and vacuum-dri...
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