Cross-linked particle plugging agent suitable for low-permeability reservoir high-water-cut horizontal well and preparation method of cross-linked particle plugging agent
A technology for horizontal wells and cross-linking agents, applied in chemical instruments and methods, drilling compositions and other directions, can solve the problems of unsatisfactory water blocking effect of plugging agents, and achieve strong water blocking ability, good erosion resistance, good water blocking effect, etc. The effect of temperature resistance
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[0032] The present invention provides a preparation method of a cross-linked granular plugging agent suitable for high water-cut horizontal wells in low-permeability reservoirs, which is specifically implemented according to the following steps:
[0033] Step 1: Add polyacrylamide and clay to normal temperature water, stir evenly, then add acrylamide and acrylic acid, stir evenly and let stand for 10 minutes to obtain reagent A;
[0034] Among them, the mass ratio of polyacrylamide, clay, water, acrylamide, and acrylic acid is 0.006:0.25:3:1:0.006;
[0035] Step 2, adding acrylic acid a into NaOH aqueous solution, stirring continuously until there is no gel, and standing for 5min to obtain reagent B;
[0036] The volume ratio of acrylic acid a and NaOH aqueous solution is 10:1; the saturation of NaOH aqueous solution is 0.75; the volume ratio of water and NaOH aqueous solution is 3:1;
[0037] Step 3: Mix the reagent A obtained in step 1 with the reagent B obtained in step 2,...
Embodiment
[0041] Step 1, add 0.3g of polyacrylamide and 12.5g of clay into 150ml of normal temperature water, stir well, then add 50g of acrylamide and 0.3g of acrylic acid, stir well and let stand for 10min to obtain reagent A;
[0042] Step 2, add 5ml of acrylic acid a to 50ml of 0.75 saturated NaOH aqueous solution, stir continuously until there is no gel, and leave it for 5min to obtain reagent B;
[0043] Step 3: Mix the reagent A obtained in step 1 with the reagent B obtained in step 2, stir until there is no precipitation, then add 0.1 g of ammonium persulfate and 0.1 g of N-N methylenebisacrylamide after standing for 3 minutes, and heat and stir at a constant temperature The instrument was heated and stirred in a water bath at 70°C for 5 minutes, and after the reaction was complete, a cross-linked particle blocking agent was obtained;
[0044] On-site implementation effect: Well X was put into production on October 2, 2012, and the average daily liquid production in the first 3 ...
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