Negative electrode for lithium secondary battery and lithium secondary battery including same
A lithium secondary battery and negative electrode technology, which is applied in the field of lithium secondary batteries, can solve problems such as deterioration of life characteristics, reduction of electrode adhesion, and increase of interface resistance
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Embodiment 1
[0073]
[0074] By adding 90.4% by weight of the first graphite-based active material (wherein artificial graphite (D50: 20 μm) and natural graphite (D50: 10 μm) are mixed in a weight ratio of 5:5), 6.0% by weight of silicon oxide (SiO x , 0<x<2, D50:5μm) of the first silicon-based active material, 0.1% by weight of SWCNT conductive material and 3.5% by weight of CMC / SBR (binder, 1.5 / 2.0 by weight) to prepare the first Negative slurry.
[0075] Prepare the second negative electrode slurry in the same manner as the first negative electrode slurry, except that the second graphite-based active material mixed with artificial graphite and natural graphite in a weight ratio of 9:1 is used instead of the first graphite-based active material .
[0076] By adding 96.4% by weight of artificial graphite with an average particle size (D50) of 20 μm to water, 0.1% by weight of SWCNT conductive material and 3.5% by weight of CMC / SBR (binder, 1.5 / 2.0) to prepare the third negative elect...
Embodiment 2 and Embodiment 3 and comparative example 1- comparative example 3
[0090] Negative electrode and button cell are manufactured in the same manner as in Example 1, except that the weight of artificial graphite and natural graphite in the first graphite-based active material (first layer) and the second graphite-based active material (second layer) is such as Table 1 below.
Embodiment 4- Embodiment 7
[0116] Negative electrode and button battery were manufactured in the same manner as in Example 1, except that the thicknesses of the first negative electrode active material layer and the second negative electrode active material layer were prepared as shown in Table 4 below.
[0117] (Evaluation method)
[0118] *Evaluation of the interfacial adhesion between the negative electrode active material layer and the current collector
[0119] The evaluation of the negative electrodes manufactured in Example 1 and Example 4-Example 7 was performed in the same manner as the evaluation of the interfacial adhesive force of Evaluation Example 1, and the evaluation results are summarized in Table 4 below.
[0120] *Evaluation of electrode volume expansion rate during negative electrode charging
[0121] The negative electrode and the button battery manufactured in Examples 1 and 4-7 were charged with a constant current of 0.1C rate at room temperature (25°C) until the voltage reac...
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