Method for extracting ginkgolic acid from waste liquid generated in ginkgo leaf extract processing process
A technology for processing waste liquid and ginkgolic acid, which is applied in the field of pharmaceutical and biopesticide raw material processing, can solve the problems of cumbersome process, time-consuming gingkgolic acid, high processing cost, etc., to expand sources, reduce adhesion, and increase energy consumption. big effect
- Summary
- Abstract
- Description
- Claims
- Application Information
AI Technical Summary
Benefits of technology
Problems solved by technology
Method used
Examples
Embodiment 1
[0027] (1) Take 100kg of ginkgo leaf processing waste liquid, filter through 100-mesh, 300-mesh, and 500-mesh filter cloths respectively three times to obtain the filtrate, and then fine-filter the filtrate with a 0.15μm ceramic membrane to obtain the fine filtrate, and then use a rotary Concentrate in the evaporator at a temperature of 85°C and a vacuum of -0.09MPa to 1 / 10 of the mass of ginkgo biloba processing waste liquid to obtain 10 kg of concentrated liquid for use;
[0028](2) Take 10kg of the concentrated solution obtained in step (1), add 5kg of silica gel powder, stir at 30r / min for 4h, stop stirring, and after standing for 1h, filter out the silica gel, add 4kg of silica gel powder to the remaining filtrate, and stir at 25r / min Stir for 3.5 hours under the condition of min, stop stirring, after standing for 1 hour, filter out the silica gel, add 3kg of silica gel powder to the remaining filtrate, stir for 3 hours under the condition of 20r / min, stop stirring, after ...
Embodiment 2
[0071](1) Take 100kg of ginkgo biloba processing waste liquid, filter it three times through 100 mesh, 300 mesh, and 500 mesh filter cloths respectively to obtain the filtrate, then fine filter the filtrate with a 0.22μm ceramic membrane to obtain the fine filtrate, and then use the rotary Concentrate in the evaporator at a temperature of 90°C and a vacuum of -0.065MPa to 1 / 20 of the mass of ginkgo biloba processing waste liquid to obtain 5 kg of concentrated liquid for use;
[0072] (2) Take 5kg of the concentrated solution obtained in step (1), add 2.5kg of silica gel powder, stir at 25r / min for 4h, stop stirring, and after standing for 1h, filter out the silica gel, add 2kg of silica gel powder to the remaining filtrate, and stir at 20r / min Stir at 15r / min for 3.5h, stop stirring, let stand for 1h, filter out the silica gel, add 1.5kg of silica gel powder to the remaining filtrate, stir for 3h at 15r / min, stop stirring, let stand for 1h, put the silica gel filter out;
[0...
Embodiment 3
[0081] (1) Take 100kg of ginkgo biloba processing waste liquid, filter it through 100 mesh, 300 mesh, and 500 mesh filter cloth three times respectively to obtain the filtrate, and then fine filter the filtrate with a 0.30μm ceramic membrane to obtain the fine filtrate, and then use the rotary The evaporator is concentrated at a temperature of 88°C and a vacuum of -0.08MPa until the quality of the ginkgo leaf processing waste liquid is 1 / 16, and 6.25 kg of the concentrated liquid is obtained for use;
[0082] (2) Take 6.25kg of the concentrated solution obtained in step (1), add 3.125kg of silica gel powder, stir at 20r / min for 4h, stop stirring, and after standing for 1h, filter out the silica gel, add 2.5kg of silica gel powder to the remaining filtrate, Stir at 20r / min for 3h, stop stirring, and after standing for 1h, filter out the silica gel, add 1.875kg of silica gel powder to the remaining filtrate, stir for 3.5h at 10r / min, stop stirring, and let stand for 1h, Filter o...
PUM
Abstract
Description
Claims
Application Information
- R&D Engineer
- R&D Manager
- IP Professional
- Industry Leading Data Capabilities
- Powerful AI technology
- Patent DNA Extraction
Browse by: Latest US Patents, China's latest patents, Technical Efficacy Thesaurus, Application Domain, Technology Topic, Popular Technical Reports.
© 2024 PatSnap. All rights reserved.Legal|Privacy policy|Modern Slavery Act Transparency Statement|Sitemap|About US| Contact US: help@patsnap.com