Method for evaluating development degree of shale microcosmic fractures based on nanoindentation experiment

A nano-indentation and developmental technology, which is applied in testing material hardness, resources, instruments, etc., can solve problems such as low elastic modulus, difficulty in completing analysis in a short period of time, even in-situ real-time monitoring, and high cost of microscopic observation methods

Active Publication Date: 2022-02-15
CHINA UNIV OF MINING & TECH (BEIJING)
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  • Abstract
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  • Claims
  • Application Information

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Problems solved by technology

However, in most cases, only a small number of cracks will cause loading bursts in the image due to fracture, and the existence of most cracks will not change the curve greatly. The apparent mechanical properties of its low hardness and low elastic modulus The properties are similar to clay, so it is often difficult to directly judge the degree of crack development of the sample through the curve shape and mechanical parameters
Moreover, the cost of microscopic observation methods is high and the cycle is long in the actual operation process, and it is difficult to meet the requirements of completing analysis in a short time or even in-situ real-time monitoring

Method used

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  • Method for evaluating development degree of shale microcosmic fractures based on nanoindentation experiment
  • Method for evaluating development degree of shale microcosmic fractures based on nanoindentation experiment
  • Method for evaluating development degree of shale microcosmic fractures based on nanoindentation experiment

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Embodiment 1

[0071] Such as figure 1 As shown, the embodiment of the present invention provides a method for evaluating the development degree of shale microscopic fractures based on nanoindentation experiments, including:

[0072] S101, performing an in-situ nanoindentation experiment, drawing a fitting curve and a theoretical curve of H / Er and Ue / Ut according to the relevant data obtained from the nanoindentation experiment, and calculating the slope of the fitting curve and the slope of the theoretical curve; wherein, Er is elastic modulus, H is contact hardness, Ue is elastic energy, Ut is total energy;

[0073] S102, calculating the vertical distance from the indentation point in the nanoindentation experiment to the theoretical curve and its average ;

[0074] S103, use the following formula to calculate the first evaluation value :

[0075]

[0076] In the formula, is the vertical distance in The number of indentation points in the interval, is the vertical distance...

specific Embodiment 1

[0134] In this example, sample 1 is used to conduct nanoindentation experiments, and the relationship images of H / Er and Ue / Ut are drawn according to the relevant data obtained in the experiment, and the proportional function is fitted ,get is 0.250. According to the type or equivalent angle of the experimental indenter, a theoretical proportional curve is made, and the proportional coefficient of the theoretical curve for =0.231.

[0135] Draw a vertical line from the indentation point to the theoretical curve, obtain the value of the vertical line segment and record it as . draw and The relation curve of the calculated is 0.01995, then is 0.63636.

[0136] Statistically obtained for 16, is 78, is 121, the first evaluation value is calculated according to the formula The value is 0.69.

[0137] according to and Calculate the second evaluation value is 0.019.

[0138] by made at intervals The polar coordinate plot of is the radius to get...

specific Embodiment 2

[0141] In this example, sample 1 is used to conduct nanoindentation experiments, and the relationship images of H / Er and Ue / Ut are drawn according to the relevant data obtained in the experiment, and the proportional function is fitted ,get is 0.226. According to the type or equivalent angle of the experimental indenter, a theoretical proportional curve is made, and the proportional coefficient of the theoretical curve for =0.231.

[0142] Draw a vertical line from the indentation point to the theoretical curve, obtain the value of the vertical line segment and record it as . draw and The relation curve of the calculated is 0.011755, then is 0.67347.

[0143] Statistically obtained is 18, for 42, is 98, and the first evaluation value is calculated according to the formula The value is 0.49.

[0144] according to and Calculate the second evaluation value is 0.005.

[0145] by made at intervals The polar coordinate plot of is the radius t...

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Abstract

The invention discloses a method for evaluating the development degree of microscopic fractures of shale based on a nanoindentation experiment. The method comprises the following steps: firstly, carrying out a nanoindentation experiment, and drawing a fitting curve and a theoretical curve of H/Er and Ue/Ut according to obtained related data; calculating a vertical distance from the indentation point to the theoretical curve and an average value of the vertical distance; calculating a first evaluation value; calculating a second evaluation value according to the slope of the fitting curve and the slope of the theoretical curve; then calculating the average value of the vertical distances within the threshold range, and calculating a third evaluation value; and finally, calculating a fracture development degree evaluation value according to the three evaluation values, evaluating the shale microcosmic fracture development degree , and judging that the larger the fracture development degree evaluation value is, the better the shale microcosmic fracture development degree is. The problems of complex internal fracture observation means, long period and difficulty in in-situ monitoring in the existing nanoindentation technology are solved, and the internal fracture of the sample can be evaluated only by acquiring displacement load data through an in-situ indentation experiment.

Description

technical field [0001] The invention relates to the technical field of drilling in soil layers or rocks, in particular to a method for evaluating the development degree of shale microscopic cracks based on nano-indentation experiments. Background technique [0002] As an important unconventional energy source, shale oil and gas can greatly improve the world's energy supply structure. Reservoir structure and mechanical properties play a vital role in the efficient extraction of shale oil and gas. [0003] At present, the research on the structure and mechanical properties of shale reservoirs is generally completed by taking cores to make shale samples for indoor experiments and micro-nano indentation mechanical testing techniques. However, in actual operation, due to the unstable chemical and physical properties of shale, coupled with the development of natural fractures and fissures, cores are easily broken and muddy, and the quality is difficult to guarantee, making it dif...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): G06F30/20G01N3/42G06Q10/06G06F111/10
CPCG06F30/20G01N3/42G06Q10/0639G06F2111/10
Inventor 杨柳张子涵孟思炜左建平何剑英徐红超夏东岳王建淇何满潮
Owner CHINA UNIV OF MINING & TECH (BEIJING)
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