A kind of slow digestion resistant dextrin and preparation method thereof
A resistant dextrin, slow technology, applied in the field of preparation of slowly digested resistant dextrin, can solve the problem of uncontrollable glycosidic bond ratio
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[0023] The invention provides a preparation method of slowly digesting resistant dextrin, comprising the following steps:
[0024] 1) mix starch and water to obtain starch milk;
[0025] 2) mixing the starch milk obtained in the step 1) with α-mesophilic amylase, and after reacting for 30 to 45 minutes, then adding pullulanase and maltotriose-generating enzyme at the same time, and performing synergistic enzymatic hydrolysis to obtain an enzymatic hydrolysis solution;
[0026] 3) carrying out the enzymatic hydrolysis solution obtained in the step 2) successively by evaporation concentration and polymerization to obtain a slowly digestible resistant dextrin crude product;
[0027] 4) Refining the slowly digestible resistant dextrin crude product obtained in the step 3) to obtain the slowly digestible resistant dextrin.
[0028] In the present invention, starch and water are mixed to obtain starch milk.
[0029] In the present invention, the starch is preferably corn starch, t...
Embodiment 1
[0052] A preparation method of slowly digesting resistant dextrin, comprising the following steps:
[0053] 1) mixing cornstarch and reverse osmosis water, adjusting the Baume degree of starch milk to be 17°Bé;
[0054] 2) First mix the starch milk obtained in step 1) with 1.2×10 8 Uα-medium temperature amylase was mixed, and after 30 minutes of reaction, 1.25×10 7 U pullulanase and 5.25 x 10 6 U maltotriose generating enzyme, pH 5.0, 52 ° C, enzymatic hydrolysis for 120 min to obtain an enzymatic hydrolysis solution with a maltotriose content of 71%;
[0055] 3) the enzymolysis solution obtained in step 2) is evaporated and concentrated in the reactor, the pressure is -0.075MPa, the temperature is 90 ° C, and the mass percentage content of evaporated to solids is 82%; add according to 0.5% of the obtained concentrated solution quality Citric acid, keep vacuum at -0.09MPa, temperature at 140°C, and react for 40min.
[0056] 4) Dissolving the slowly digested resistant dextr...
Embodiment 2
[0059] A preparation method of slowly digesting resistant dextrin, comprising the following steps:
[0060] 1) mixing cornstarch and reverse osmosis water, adjusting the Baume degree of starch milk to be 16°Bé;
[0061] 2) First mix the starch milk obtained in step 1) with 2.4×10 8 Uα-medium temperature amylase was mixed, reacted for 45min, and then added 2×10 7 U pullulanase and 4.5 x 10 6 U maltotriose generating enzyme, pH 5.3, 54 ℃, enzymatic hydrolysis for 180 min, to obtain an enzymatic hydrolysis solution with a maltotriose content of 72%;
[0062] 3) The enzymolysis solution obtained in step 2) was evaporated and concentrated in the reaction kettle, the pressure was -0.06MPa, the temperature was 95°C, and the mass percentage content of evaporated to solids was 83%; add according to 1.25% of the obtained concentrated solution quality Phosphoric acid, keep vacuum -0.06MPa, temperature 148℃, and react for 32min.
[0063] 4) Dissolving the slowly digested resistant dex...
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