Toothpaste containing fibroin and preparation method thereof
A technology of silk protein and silk protein powder, which is applied in the field of toothpaste containing silk protein and its preparation, can solve the problems of toxicity and side effects, and achieve the effects of low cost, enhanced cleaning effect, and gum protection
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[0044] Preparation of silk fibroin protein powder: take silkworm cocoon shells and wash them, and use saturated sodium carbonate solution to boil for 50 minutes to degumming. Dry the degummed cocoons and dissolve them with 8mol / L lithium bromide solution or calcium chloride solution. The solution is dialyzed to remove impurities, concentrated and then freeze-dried to obtain silk fibroin powder.
[0045] Preparation of sericin protein powder: take silkworm cocoon shells and wash them, and use deionized water to boil for 30 minutes to extract sericin solution. The sericin solution is concentrated and then freeze-dried to obtain sericin protein powder.
[0046] Prepare silk fibroin powder, colored cocoon sericin powder and white cocoon sericin powder respectively according to the above method, and dissolve the aforementioned three silk protein powders in water to prepare silk protein solution samples with a mass percentage concentration of 0.1%, namely Silk fibroin powder aqueo...
Embodiment 1
[0057] Taking the total amount of material as 100g, the toothpaste containing silk protein in the present embodiment comprises the following raw materials:
[0058] Sufficient cocoon shell, 20g of sorbitol, 45g of calcium hydrogen phosphate, 4.5g of polyethylene glycol, 2g of sodium lauryl sulfate, 2g of sodium lauroyl sarcosinate, 1g of essence, 0.5g of fiber Vegetarian Gum, 0.5g of Crinkle Carrageen, 0.2g of Monosodium Phosphate, 0.8g of Sodium Pyrophosphate, 0.5g of Sodium Monofluorophosphate, 0.05g of Methylparaben, 0.1g of Propylparaben .
[0059] The preparation method of above-mentioned toothpaste comprises the following steps:
[0060] (1) Take silkworm cocoon shells and wash them, and use saturated sodium carbonate solution to boil for 50 minutes for degumming. Dry the degummed cocoons and dissolve them with 8mol / L lithium bromide solution or calcium chloride solution. The solution is dialyzed to remove impurities, concentrated and then freeze-dried to obtain silk ...
Embodiment 2
[0065] The preparation process and the amount of materials added are the same as in Example 1, except that the amount of silk fibroin powder added in the toothpaste containing silk protein prepared in this example is 1 g.
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