Shuanghuanglian effervescence tablet and its preparation
A technology of Shuanghuanglian and effervescent tablets, which can be used in pharmaceutical formulations, medical preparations containing active ingredients, and drug delivery, etc., can solve problems such as waste of resources and low extraction rate of active ingredients.
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Embodiment 1
[0015] 1. Prescription Honeysuckle 750g, Scutellaria baicalensis 750g, Forsythia 1500g
[0016] Take the prescribed amount of medicinal materials, dry them at low temperature, pulverize them with a Bailey micro-powder machine, and set aside. Take Scutellaria baicalensis powder, add water and decoct three times, the first time for 2 hours, the second and third times for 1 hour each, combine the decoction, filter, concentrate the filtrate to an appropriate amount, add 2mol / L hydrochloric acid solution to the concentrated solution at 80°C, and adjust the pH value to 1.0-2.0, keep warm for 1 hour and then stand for 24 hours, filter, add 6-8 times the amount of water to the precipitate, adjust the pH value to 7.0-7.5 with 40% sodium hydroxide solution, add the same amount of ethanol, stir to dissolve , filtered. The filtrate was adjusted to pH 2.0 with 2mol / L hydrochloric acid solution, kept at 60°C for 30 minutes, allowed to stand for 12 hours, filtered, and the precipitate was w...
Embodiment 2
[0018] 1. Prescription Honeysuckle 750g, Scutellaria baicalensis 750g, Forsythia 1500g
[0019] Take the prescribed amount of medicinal materials, dry them at low temperature, pulverize them with a Bailey micro-powder machine, and set aside. Take Scutellaria baicalensis powder, add water and decoct three times, the first time for 2 hours, the second and third times for 1 hour each, combine the decoction, filter, concentrate the filtrate to an appropriate amount, add 2mol / L hydrochloric acid solution to the concentrated solution at 80°C, and adjust the pH value to 1.0-2.0, keep warm for 1 hour and then stand for 24 hours, filter, add 6-8 times the amount of water to the precipitate, adjust the pH value to 7.0-7.5 with 40% sodium hydroxide solution, add the same amount of ethanol, stir to dissolve , filtered. The filtrate was adjusted to pH 2.0 with 2mol / L hydrochloric acid solution, kept at 60°C for 30 minutes, allowed to stand for 12 hours, filtered, and the precipitate was w...
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