Modifier for increasing impact resistance of polyvinyl chloride
A technology of impact resistance and polyvinyl chloride, which is applied in the field of modifiers for improving the impact resistance of polyvinyl chloride, can solve problems such as poor impact resistance, and achieve improved toughness, excellent toughening effect, and improved uniform dispersion. Effect
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Embodiment 1
[0018] Preparation of seed emulsion: In a 1000ml three-necked flask equipped with a stirrer and a reflux condensing device, nitrogen protection was introduced, and the temperature was kept at 60°C. 400g of deionized water, 0.20g of sodium dodecylsulfonate, and 20g of butyl acrylate were added. 0.20g of potassium peroxodisulfate was stirred, and a pre-emulsion consisting of 200g of BA monomer, 60g of deionized water, and 0.9g of SLS emulsifier was added dropwise, and polymerized for 2 hours to obtain a seed emulsion.
[0019] Preparation of pre-emulsion: Weigh 300g of BA monomer, take 30g of deionized water, 0.6g of SLS emulsifier, 0.3g of CHP initiator, 2.0g of triethylene glycol triacrylate, and emulsify with an emulsifier to obtain a pre-emulsion.
[0020] Seed growth: Add 400g deionized water and 0.20g sodium dodecylsulfonate into a three-necked flask, stir, pass nitrogen gas to remove oxygen at 60°C, add 0.40g Diaobaikuai, 10g seed emulsion, and drop pre-emulsion , add 0.2...
Embodiment 2
[0023] Preparation of seed emulsion: In a 1000ml three-necked flask equipped with a stirrer and a reflux condensing device, nitrogen protection was introduced, and the temperature was kept at 60°C. 400g of deionized water, 0.20g of sodium dodecylsulfonate, and 20g of butyl acrylate were added. 0.20g of potassium peroxodisulfate was stirred, and a pre-emulsion consisting of 200g of BA monomer, 60g of deionized water, and 0.9g of SLS emulsifier was added dropwise, and polymerized for 2 hours to obtain a seed emulsion.
[0024] Preparation of pre-emulsion: Weigh 300g of BA monomer, take 45g of deionized water, 1.5g of SLS emulsifier, 3.0g of CHP initiator, 3.0g of allyl acrylate grafting agent, and emulsify with an emulsifier to obtain a pre-emulsion.
[0025] Seed growth: Add 500g deionized water and 0.20g sodium dodecylsulfonate into a three-necked flask, stir, pass nitrogen gas to remove oxygen at 60°C, add 0.40g Diaobai block, 10g seed emulsion, and then add pre-emulsification...
Embodiment 3
[0028] Preparation of seed emulsion: In a 1000ml three-neck flask equipped with a stirrer and a reflux condensing device, nitrogen protection was introduced, the temperature was kept at 80°C, 400g of deionized water, 1.0g of sodium dodecylsulfonate, and 20g of butyl acrylate were added. 0.20g of potassium peroxodisulfate was stirred, and a pre-emulsion consisting of 200g of BA monomer, 60g of deionized water, and 0.9g of SLS emulsifier was added dropwise, and polymerized for 2 hours to obtain a seed emulsion.
[0029] Preparation of pre-emulsion: Weigh 300g of BA monomer, take 30g of deionized water, 1.5g of SLS emulsifier, 0.90g of CHP initiator, 4.5g of triethylene glycol triacrylate, and emulsify with an emulsifier to obtain a pre-emulsion.
[0030] Seed growth: Add 600g deionized water and 0.20g sodium dodecylsulfonate into a three-necked flask, stir, pass nitrogen gas to remove oxygen at 60°C, add 0.40g Diaobai block, 10g seed emulsion, and then drop pre-emulsified soluti...
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