Method for preparing conducting fiber and product thereof
A technology of conductive fibers and conductive components, which is applied in fiber processing, textiles and papermaking, etc., can solve the problems of conductive high polymers restricting direct spinning applications, and achieve the effects of non-shedding conductivity, soft hand feeling and low resistivity
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preparation example Construction
[0026] The preparation method of the conductive fiber of the present invention is further characterized in that 5-20 wt% of the matrix fiber is added to the formula for configuring the conductive coating solution. This formula design of dissolving an appropriate amount of matrix fiber in the conductive coating liquid can increase the viscosity of the conductive coating liquid on the one hand, and can strengthen the bonding fastness between the coating layer and the matrix fiber on the other hand, which is better Improve the efficiency of surface dissolution-coating treatment.
[0027] The conductive fiber manufactured by the preparation method of the present invention has excellent electrical conductivity, and its volume specific resistance range can reach 10 0 Ω.cm~10 8 Ω.cm order of magnitude, and basically does not reduce its mechanical and physical properties, and at the same time feels soft, comfortable to wear when used in special clothing, and has excellent performance...
Embodiment 1
[0030] 1. Conductive component pretreatment. The conductive component is carbon black, which is pretreated by dry mixing method. Add carbon black into the high-mixer, stir at a high speed of 4000rpm for 10min, and heat up to 70°C. Spray the titanate coupling agent in the form of carbon black; first stir at a low speed of 1000rpm for 5 minutes, then stir at a high speed of 6000rpm for 10 minutes, and then the treated carbon black can be obtained.
[0031] 2. Configure the conductive coating solution, and configure the coating solution according to the following weight percentage formula:
[0032] Purified water 25%,
[0033] Formic acid 50%,
[0034] Carbon black 25%;
[0035] 3. To manufacture conductive fibers, apply the above-mentioned coating solution evenly on the surface of the polyamide fiber to be treated on a continuous coating machine at a speed of 5m / min; then wash with hot water at 70°C to remove the solvent remaining in the fiber. The surface dissolution-coated ...
Embodiment 2
[0038] 1. Pretreatment of conductive components, carbon black is selected as the conductive component, and when carbon black is pretreated by dry mixing method, carbon black is added into the high-mixer, stirred at a high speed of 4000rpm for 10min, and heated to 80C to Spray into the titanate coupling agent in mist form. Stir at 2000rpm at low speed for 10min first, then stir at 7000rpm at high speed for 30min to obtain the treated carbon black.
[0039] 2. Configure the conductive coating solution, and configure the coating solution according to the following weight percentage formula:
[0040] Phenol 40%,
[0041] Tetrachloroethane 40%,
[0042] Carbon black 20%.
[0043] 3. To manufacture conductive fibers, use a fiber continuous coating machine to evenly coat the coating solution on the surface of the polyester fiber to be treated at a speed of 4m / min, then wash with hot water at 80°C to remove the solvent remaining in the fiber, and use 60 ℃ hot air drying to continu...
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