Process for preparing optical orientation film
A photo-alignment film and photo-alignment technology, applied in optics, nonlinear optics, instruments, etc., can solve the problems of loss of alignment state, structural obstruction, inability to maintain liquid crystal alignment function, etc., and achieve the effect of excellent stability
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[0014] The material for photo-alignment films used in the production method of the present invention contains a dichroic dye having two or more polymerizable groups in one molecule. Among the dichroic dyes having two or more polymerizable groups in one molecule, the so-called dichroic dyes are dyes in which the ability to absorb light as a chromophoric group differs depending on the direction of the electric vector of polarized light. Among dichroic dyes, there are, for example, anthraquinones, azos, quiphthalones, and northern dyes. Among them, azo dyes or anthraquinones show particularly excellent photo-orientability by irradiating polarized light, so Especially ideal. The azo dye or anthraquinone dye before introducing the polymerizable group is not particularly limited as long as it can be used as a dichroic dye.
[0015] The dichroic dye having a polymerizable group used in the present invention can be, for example, prepared by making a dichroic dye having a hydroxyl gro...
Embodiment 1~8
[0054] A photo-alignment film was formed using the materials for photo-alignment films of the compounds obtained in Synthesis Examples 1 to 6, and the orientation, charge retention, and durability of liquid crystals were evaluated. The specific test process is as follows. (Manufacturing method of photo-alignment film) a-1. Preparation of material solution for photo-alignment film (for photopolymerization)
[0055] To 99 parts by mass of the compound obtained in the synthesis example and the comparative synthesis example, 1 part by mass of the photopolymerization initiator "Irugakiua-651" (manufactured by Tibagaigie Co., Ltd.) was added and dissolved in dimethylformamide to obtain the nonvolatile component 5 mass % solution. This solution was filtered through a 0.1 μm filter to obtain a material solution for a photo-alignment film. a-2. Preparation of material solution for photo-alignment film (for thermal polymerization)
[0056] To 99 parts by mass of compounds obtained in...
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