Preparation for fish gold and its preparing method
A kind of preparation, fish gold technology, applied in antiviral agents, pharmaceutical formulas, medical preparations containing active ingredients, etc., can solve the problem of insufficient utilization of raw materials, achieve obvious antiviral and inhibitory effects, antipyretic effects, obvious effect
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Embodiment 1
[0022] (1) soak Houttuynia cordata and honeysuckle flowers with a weight ratio of 4:1 for 2 hours;
[0023] (1) Extract the volatile components of Houttuynia cordata and Flos Lonicerae by distillation to obtain a distillation extract equivalent to 15% of the total weight of medicinal materials;
[0024] (1) adding water to extract Houttuynia cordata and honeysuckle dregs extracted by distillation twice, combine the extracts, filter, concentrate until the temperature is 75°C and the relative density is 1.12, add 3 times the amount of 95% ethanol, Stir fully at a temperature of 40°C, cool and place for 2 hours, filter, wash the residue twice with 60% ethanol, combine the alcohol liquid, recover ethanol, and then add 5 times more ethanol with an amount of 90% or more, at a temperature of 40°C The mixture was fully stirred under cooling, and left to stand for 2 hours after cooling, the supernatant was collected by filtration, and ethanol was recovered from the filtrate. Add 3 tim...
Embodiment 2
[0027] (1) soak Houttuynia cordata and honeysuckle flowers with a weight ratio of 4:2 for 2 hours;
[0028] (2) extract the volatile components of Houttuynia cordata and honeysuckle by distillation to obtain a distillation extract of 15% of the total weight of medicinal materials; the distillation extract is clathrated with hydroxypropyl-β-cyclodextrin to form hydroxypropyl Base-β-cyclodextrin inclusion complex.
[0029] (3) Extract Houttuynia cordata and honeysuckle dregs extracted by distillation twice with water, combine the extracts, filter, concentrate until the relative density is 1.11 at a temperature of 70°C-80°C, add 3 times the amount of 90 % ethanol, fully stirred at a temperature of 40°C, cooled and placed for 2 hours, filtered, the residue was washed twice with 60% ethanol, the alcohol liquid was combined, ethanol was recovered, and 5 times more than 90% ethanol was added, Stir well at a temperature of 40°C, let stand for 2 hours after cooling, collect the supern...
Embodiment 3
[0032] (1) soak Houttuynia cordata and honeysuckle flowers with a weight ratio of 4:3 for 2 hours;
[0033] (2) Extract the volatile components of Houttuynia cordata and Flos Lonicerae by distillation to obtain a distillation extract of 15% of the total weight of medicinal materials;
[0034] (3) Extract Houttuynia cordata and honeysuckle dregs extracted by distillation twice with water, combine the extracts, filter, concentrate until the relative density is 1.10 when the temperature is 70°C, add 3 times the amount of 85% ethanol , fully stirred at a temperature of 35°C, cooled and placed for 2 hours, filtered, the residue was washed twice with 55% ethanol, the alcohol liquid was combined, the ethanol was recovered, and 5 times more than 90% ethanol was added. Stir well at high temperature, let stand for 2 hours after cooling, filter the supernatant, and recover ethanol from the filtrate. Add 3 times the amount of distilled water, adjust the pH value to 7.0, heat to 100°C, le...
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