Process of modified starch by powder milling mechanical forec chemistry method
A mechanochemical and starch technology, applied in the field of starch modification, can solve the problems of insufficient use of mechanochemical methods, low pulverization efficiency, and invariance, and achieve enhanced binding capacity, biodegradation speed and biodegradation. The effect of improving the degree and good application prospect
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Embodiment 1
[0019] Take by weighing 200g tapioca starch (dry basis) and 2400g ceramic ball milling medium (d=7mm) respectively and pour in the plastic ball mill jar, then measure 320ml dehydrated ethanol and add in the jar, cover and place the rotating speed of On the 170rpm ball mill, turn on the switch for ball milling. Shut down and observe every 20 hours, and add 20ml of absolute ethanol. After ball milling for 150 hours, stop grinding, take out the starch milk and place it in a storage container, vacuum filter to remove ethanol and recover, dry the obtained wet product of grinding at 40°C, grind, pass through a 200-mesh sieve, and obtain Micronized tapioca starch products.
[0020] Table 1. Changes in median diameter and specific surface area of cassava starch particles after ball milling
[0021] Milling time (hours) particle median diameter (μm) specific surface area (m 2 .g -1 )
[0022] 0 10.78 0.444
[0023] 150 1.38 4.407
[0024] The results in Table ...
Embodiment 2
[0026] Weigh 100g of potato starch (on a dry basis) and 1005g of ceramic balls respectively and pour them into a plastic ball mill jar, wherein the ceramic balls with a diameter of 3mm and 9mm are half and half. Then measure 147ml absolute ethanol and add in the jar, put on the ball mill that rotating speed is 150rpm after covering and tightening, close switch and carry out ball milling. After 16 hours, shut down and observe once, and add 10ml of absolute ethanol. Stop grinding after 25 hours of ball milling, take out the starch milk and place it in a storage container, remove ethanol by vacuum suction filtration and recover, dry the obtained wet product of grinding at 50°C, grind, and pass through a 200-mesh sieve to obtain Micronized potato starch products.
[0027] Observing the starch sample after ball milling for 25 hours with a polarizing microscope, the polarized cross of the granules has completely disappeared, indicating that the crystal structure of the starch has c...
Embodiment 3
[0029]Weigh 200g of potato starch (on a dry basis) and 2240g of ceramic balls and pour them into a plastic ball mill jar, wherein the mass ratio of ceramic balls with a diameter of 5mm and 10mm is 2:1. Then measure 270ml absolute ethanol and add in the jar, put on the ball mill that rotating speed is 100rpm after covering and tightening, close switch and carry out ball milling. After 20 hours, shut down and observe once, and add 50ml of absolute ethanol. Stop grinding after ball milling for 75 hours, take out the starch milk and place it in a storage container, remove ethanol by vacuum suction filtration and recover, dry the obtained wet product of grinding at 45°C, grind, and pass through a 200-mesh sieve to obtain Micronized potato starch products.
[0030] Table 2. The change of apparent viscosity of mung bean starch before and after ball milling for 200h with temperature
[0031] Milling time Weight gain after moisture absorption Dissolving at 40°C Swelli...
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