Medicine composition for treating cervical spondylosis and its preparing method
A composition and technology for cervical spondylosis, applied in the field of pharmaceutical compositions for the treatment of cervical spondylosis, can solve the problems of drugs and pharmaceutical preparations for treating cervical spondylosis, and achieve the effect of clear drug effect, strong controllability and stable quality
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Embodiment 1
[0037] The extraction of embodiment 1 pharmaceutical raw material of the present invention
[0038] a, the preparation of Rhizoma Chuanxiong alkaloid: get the coarse powder of Rhizoma Chuanxiong medicinal material, soak, percolate with pH value 2~3 acid water, in per Kg medicinal material, percolation rate is 4~5ml / min, collect percolation liquid, pass through large Porous adsorption resin, the eluent passes through the strong acidic cation exchange resin, elutes with a certain concentration of hydrochloric acid, collects the eluent, concentrates, the concentrated solution passes through the macroporous adsorption resin, collects the column liquid, and dries to obtain the total alkaloids of Ligusticum chuanxiong ;
[0039] b. Preparation of total flavonoids of Pueraria lobata: take Pueraria lobata, extract with reflux of 50% ethanol, recover ethanol from the ethanol extract under reduced pressure, filter, pass through an adsorption resin column, elute with 70% ethanol, collect...
Embodiment 2
[0040] The extraction of embodiment 2 pharmaceutical raw materials of the present invention
[0041] a. Chuanxiong alkaloids: take the coarse powder of Chuanxiong medicinal materials, soak and percolate with acid water with a pH value of 3, based on each Kg of medicinal materials, the percolation rate is 5ml / min, collect the percolating liquid, pass through the macroporous adsorption resin, and elute The solution is then passed through a strong acidic cation exchange resin, eluted with a certain concentration of hydrochloric acid, the eluate is collected, concentrated, the concentrated solution is passed through a macroporous adsorption resin, the column liquid is collected, and dried to obtain the total alkaloids of Rhizoma Chuanxiong;
[0042] b. Total flavonoids of kudzu root: take kudzu root, reflux extraction with 50% ethanol, recover ethanol from the ethanol extract under reduced pressure, filter, pass through an adsorption resin column, elute with 30% ethanol, collect th...
Embodiment 3
[0043] Embodiment 3 Extraction of pharmaceutical raw materials of the present invention
[0044] a. Chuanxiong alkaloids: take the coarse powder of Chuanxiong medicinal materials, soak and percolate with acid water with a pH value of 2, in terms of each Kg of medicinal materials, the percolation rate is 4ml / min, collect the percolating liquid, pass through the macroporous adsorption resin, and elute The solution is then passed through a strong acidic cation exchange resin, eluted with hydrochloric acid, the eluate is collected, concentrated, the concentrated solution is passed through a macroporous adsorption resin, the column liquid is collected, and dried to obtain the total alkaloids of Rhizoma Chuanxiong;
[0045] b. Total flavonoids of kudzu root: take kudzu root, reflux extraction with 90% ethanol, recover ethanol from the ethanol extract under reduced pressure, filter, pass through an adsorption resin column, elute with 90% ethanol, collect ethanol eluate, recycle ethano...
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Abstract
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