Multifunctional reactor for preparing ionic liquid

A reactor and reaction technology, applied in chemical/physical/physical-chemical stationary reactors, chemical instruments and methods, mixers with rotary stirring devices, etc., can solve the problems of synthesis and preparation without ionic liquids, and achieve savings The effect of equipment investment and operating costs, cost reduction and utilization improvement

Active Publication Date: 2006-11-08
INST OF PROCESS ENG CHINESE ACAD OF SCI
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Problems solved by technology

The patent "Multifunctional Chemical Reactor", authorized announcement number: CN22678564 patent, relates to a reactor for chemical experiments, bu

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  • Multifunctional reactor for preparing ionic liquid

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Embodiment Construction

[0029] See figure 1 . One-pot reactor, the tank body is a jacketed tank body, the cavity of the tank body is the reaction chamber 1, and the hollow interlayer formed by the double-layer tank body wall is the jacket 5; a jacket medium is opened on the jacket 5 Inlet 7, a jacket medium outlet 4 is opened at the lower part of the jacket, a liquid feed port 10 is opened at the upper part of the tank body, and a vacuum tube 8 and a vacuum filter tube 9 are installed, and the air inlet of the vacuum filter tube is in the filter screen Above, the gas feed pipe 11, and the air outlet of the gas feed pipe is in the material below the filter screen, temperature sensor 13, pressure sensor 14, sight glass 15, condensate return pipe 16; The high-speed motor 12 is installed on the top of the tank body, and the stirring paddle is below the filter screen; a manhole or a hand hole 2 and a solid material outlet 3 are opened at the bottom of the tank body; a sampling port 20 is opened at the bo...

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Abstract

The present invention belongs to the field of ionic liquid preparing reactor, and is especially one multifunctional ionic liquid preparing reactor. The reactor is one kettle type or one horizontal reactor, which has a sandwiched reactor body with medium inlet and outlet, gaseous material inlet pipe, liquid material inlet pipe, vacuum pipe, vacuum suction filtering pipe, slurry stirring motor, temperature sensor, pressure sensor, sight glass, condensate return pipe, solid material outlet, bottom sampling port, etc. The present invention makes it possible to complete multiphase reaction or homogeneous reaction and subsequent product separation and purification, and has high reaction conversion rate, high equipment utilizing rate, less material conveying links and less impurity introduction.

Description

technical field [0001] The invention belongs to the field of reactors for preparing ionic liquids, in particular to a multifunctional reactor for synthesizing and preparing ionic liquids. Background technique [0002] Room Temperature Ionic Liquids (RTILs) are salts composed of organic cations and inorganic or organic anions that are liquid at or near room temperature, referred to as ionic liquids. Because of its excellent characteristics such as low melting point (always in a liquid state at room temperature), low vapor pressure, and low volatility, it has very good industrial application prospects, and its application fields are becoming more and more extensive, involving organic synthesis, extraction and separation, electrochemistry, biological Catalytic processes etc. [0003] At present, most of the ionic liquids are synthesized and purified on a small scale in the laboratory, the raw materials are expensive, the operation is complicated, the cost of raw materials is h...

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Application Information

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IPC IPC(8): B01J19/00B01F7/18B01J19/18
Inventor 张锁江张香平张延强李春山陈玉焕
Owner INST OF PROCESS ENG CHINESE ACAD OF SCI
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