Controlled release analgesic suspensions
A medicament and liquid technology, applied in the field of controlled release pharmaceutical preparations, can solve the problems of increasing the overall cost and product production cycle, and being unable to provide immediate release dosage forms for users.
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[0054] The coated active ingredient granules can be prepared by any suitable method known in the art. Suitable granule formation and coating methods include: high shear granulation, fluidized bed granulation, e.g. drum granulation, fluidized bed coating, agglomeration, spray drying, spray coagulation, etc., and see for example Pharmaceutical DosageForms: Tablet Vol. 3, edited by Herbert A. Lieberman and Leon Lachman, Chapters 2, 3 and 4 (1982). In one embodiment, the particles coated with the controlled-release composition have an average particle size of about 20-400 microns, such as about 50-300 microns.
[0055] The medicaments of the invention may contain one or more active ingredients. Suitable active ingredients range widely and include, but are not limited to: pharmaceuticals, minerals, vitamins and other health products, oral care agents, fragrances, and mixtures thereof. Suitable medications include: analgesics, anti-inflammatories, anti-arthritics, narcotics, antih...
Embodiment 1
[0094] Embodiment 1: Preparation of controlled-release coating solution
[0095] Preparation of coating solution: methacrylate copolymer, "Eudragit L-100" from Rohm Parma, Inc., and cellulose acetate were dispersed in a solvent containing 98% acetone and 2 %water.
[0096] The resulting coating solution contained 7.6% cellulose acetate, 0.4% methacrylate copolymer, 90.2% acetone and 1.8% water, based on the total weight of the wet coating solution.
[0097] The corresponding solids levels were 95.00% cellulose acetate and 5.00% methacrylate copolymer, based on the total weight of the dry coating solution.
Embodiment 2
[0098] Example 2: Preparation of coated active ingredients
[0099] Preparation of Ibuprofen Premix: Mix Ibuprofen USP powder with colloidal silicon dioxide to form the following ibuprofen premix:
[0100] Content % by weight*
[0101] Colloidal silica 2.00%
[0102] Ibuprofen USP 98.00%
[0103] *Based on total weight of ibuprofen premix
[0104] Preparation of coated ibuprofen granules: use the wet controlled release coating solution prepared in Example 1 to coat the ibuprofen mixture prepared above, and the coating speed is about 20.0g / min, using Clatt-GPCG- 5 / 9 Wurster fluidized bed coating equipment, the product temperature is about 29-32 ℃. The obtained coated ibuprofen granules contain about 20% of the controlled-release coating based on the total dry weight of the ibuprofen granules plus the controlled-release coating.
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