Synthetic fuel comprising coal dust, water and a reactive organic compound, and a process for making such synthetic fuel
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example 1
[0057] Technique
[0058] A sample was prepared. The sample mixed 1 lb. of Ciba Magnafloc 155 with 2000 pounds of ground pond creek clean coal, ground to a particle size where about 90% of the particles were less than 50 microns. The Magnafloc 155 was mixed with water until fully hydrated--removal time is 3 to 10 minutes. After removing it was added to the coal dust and fully mixed. The mixture was then compacted using a 2 ton press.
[0059] The sample prepared above were compared with Pond Creek Clean Coal base coal, i.e. raw untreated coal, and the following results obtained:
1 Pond Creek Coal Inventive Sample % Moisture 9.06 less than 1.00 % Sulfur 0.94 1.03 BTU / lb 12333 13452
example 2
[0060] An analysis was made of the synthetic fuel sample at a loading of 5% to the amount of coal dust with a small amount of water.
[0061] The process blended the parent coal with a binder to make a synthetic fuel product. Technical information was then obtained from a series of tests on the synthetic fuel and the parent coal and binder described below.
[0062] Objective
[0063] The objective of performing analytical tests summarized herein was to determine if the process used to manufacture the synthetic fuel had significantly altered the chemical structure of performing certain types of analyses. The tests performed on the samples were selected due to their ability to determine differences in chemical structure and relatively common use of the tests.
[0064] Procedures
[0065] Portions of the parent coal, organic chemical, and synthetic fuel products were obtained and prepared for analysis. A series of tests, including Fourier transformed infrared (FTIR) analysis, thermo-gravimetric analy...
example 3
[0089] Technique
[0090] Two additional samples were prepared. The first sample mixed one pound of Lorama starch JK270 with 2000 pounds of coal dust using the technique of Example 1. A second sample was made using a mixture of 1 / 2 pound of CIBA Magnafloc 155 and 1 / 2 pound of Lorama starch JK270 with a similar amount of coal dust to the first sample.
[0091] Similar tests as described above were conducted.
[0092] Sample 1
[0093] The FTIR spectrum for the additive was run. A comparison of the spectra for the fuel product with that determined for a corresponding simple mixture of the parent coal and additive was made. Computer-measured areas of key absorption peaks were listed and compared for the fuel product / simple mixture.
[0094] Comparison of the spectra of the samples showed significant variation in FTIR measured peak areas relative to the parent materials at the spectral location associated with aromatic CH, carbon-oxygen bonding, carbonyl, ketones, carboxyl groups, thiophenes, heterocy...
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