Method for forming a displacement tin alloy plated film, displacement tin alloy plating bath and method for maintaining a plating performance
a technology of displacement tin alloy and plating bath, which is applied in the direction of liquid/solution decomposition chemical coating, coating, printed circuit manufacturing, etc., can solve the problems of lowering solderability, lead-free solders are inferior in solderability to tin-lead alloys, and adverse influence on solder bondability, etc., to achieve excellent uniformity, maintain the plating performance of the plating bath, and good solderability
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[0054]Examples and Comparative Examples are shown to more particularly illustrate the present invention, which should not be construed as limited to the following Examples.
experimental examples 1 to 3
[0058]A displacement tin alloy plating bath having the following bath composition 4 was provided and used both for a low temperature bath and a high temperature bath. As a test piece, there was used a rolled copper sheet on which a copper film having a thickness of about 10 μm had been formed by copper sulfate electroplating. The test piece was subjected to degreasing and acid cleaning, followed by immersion (one minute) in a low temperature displacement tin alloy plating bath (30° C.) and subsequent immersion (15 minutes) in a high temperature displacement tin alloy plating bath (60° C.).
[0059]This plating operation was repeated, under which thiourea and silver methansulfonate were, respectively, added to make such concentrations as indicated in Tables 3 to 5 in every increment of 1 g / L of a copper concentration in the low temperature displacement tin alloy plating bath and the high temperature displacement tin alloy bath. In Experimental Example 1, the concentrations of thiourea a...
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