Coffee Treatment Method
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[0053]An amount of coffee extraction residue material was mixed with water to form a slurry (10% by weight solids) and passed into a plug flow reactor. The slurry was heated to 230° C. for 6 minutes. After this thermal hydrolysis step, the solids were extracted (by centrifuging) from the slurry and discarded to leave a liquid hydrolysate 1 (see the flow chart in FIG. 1).
[0054]The liquid hydrolysate 1 was then mixed in a mixing step 3 with sufficient ethanol (food-grade) to form an 80% v / v ethanolic solution 5. The mixing step 3 was performed on a continuous liquid hydrolysate 1 stream passing from the plug flow reactor.
[0055]The ethanolic solution 5 was allowed to cool to encourage the MOS fraction to precipitate out. After precipitation the suspension was centrifuged in a separation step 7. The separation step 7 produced a supernatant 9 which was discarded and a precipitate 11.
[0056]The precipitate 11 was then re-dissolved in minimal water and freeze-dried in a finishing step 13. T...
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