Colouring of keratinous fibers using a pretreatment comprising an iron salt and a colour developer comprising hydrolysable tannin
a technology of keratinous fibers and pretreatment, which is applied in the direction of dyeing process, hair cosmetics, chemistry apparatus and processes, etc., can solve the problems of cumulative damage, damage to hair, and no control to the consumer
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example 1
Demonstration of the Effect of Buffer on Colour Development
[0058]White hair switches were incubated in the following pre-treatment compositions described below for 45 minutes[0059]Sample 1: Untreated[0060]Sample 2: With pre-treatment composition comprising—per 100 ml[0061](i) Ferrous chloride—3.8 g[0062](ii) Sodium dithionite—0.9 g[0063](iii) Propylene Carbonate—20 g[0064]Made up to 100 ml using deionised water[0065]Sample 3: With pre-treatment composition comprising—per 100 ml[0066](i) Ferrous chloride—3.8 g[0067](ii) Sodium dithionite—0.9 g[0068](iii) Propylene carbonate—20 g[0069](iv) 1.5 M Propionate buffer pH 5 (30 ml)[0070]Made up to 100 ml using deionised water
[0071]The hair switches were then washed with shampoo, rinsed with water and dried.
[0072]The hair switches were then incubated in the colour developer solution (described above) for 30 minutes. The switches were again washed well with a shampoo, rinsed with water and dried before the colour intensity was measured using ...
example 2
Effect of Time of Mixing the Buffer on the Colour Development
[0075]The three components of the pre-treatment composition were as follows:[0076](a) 3.8 g Ferrous chloride+0.9 g Sodium dithionite made up to 50 ml using deionised water[0077](b) 1.5 M Propionate buffer pH 5.0 (30 ml)[0078](c) Propylene carbonate—20 ml.
(a), (b) and (c) were mixed together and kept for different time intervals 0 mins, 60 mins, 180 mins, 360 mins and 24 hrs before the experiment was conducted.
[0079]Predominantly white hair switches were dipped in the pre-treatment compositions for 60 minutes and then washed with shampoo, rinsed with water and dried.
[0080]They were then incubated in the colour developer solution (described above) for 30 minutes. The switches were washed well with shampoo, rinsed with water and dried before the colour intensity was measured using sigma scan software. The colour intensity was read on a 0-255 scale 0 refers to black and 255 refers to white. The data is presented below in Table...
example 3
Effect of Nature of Iron Salt on Colour Development
[0090]Predominantly white hair switches were incubated in the pre-treatment solution comprising different iron salts (examples from EP0327345) as detailed below for 60 minutes.[0091]Sample 12: Untreated[0092]Sample 13: Pre-treatment Composition comprising per 100 ml[0093](i) Ferrous ammonium sulphate—8.5 g[0094](ii) Sodium dithionite—0.9 g[0095](iii) Propylene carbonate—20 g[0096](iv) 1.5 M Propionate buffer pH 5.0 (30 ml)[0097]Made up to 100 ml using deionised water[0098]Sample 14: Pre-treatment Composition comprising—per 100 ml[0099](i) Ferric Ammonium Sulphate—8.0 g[0100](ii) Sodium dithionite—0.9 g[0101](iii) Propylene carbonate—20 g[0102](iv) 1.5 M Propionate buffer pH 5.0 (30 ml)[0103]Made up to 100 ml using deionised water[0104]Sample 15: Pre-treatment Composition comprising—per 100 ml[0105](i) Ferrous chloride—3.8 g[0106](ii) Sodium dithionite—0.9 g[0107](iii) Propylene carbonate—20 g[0108](iv) 1.5 M Propionate buffer pH 5.0...
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