Application of magnolia bark and its active ingredient in preparing medicament for treating tumour stem cell
A technology of tumor stem cells and effective components, which is applied to the application field of Magnolia officinalis and its effective components in the preparation of medicines for treating tumor stem cells, can solve the problems such as not being discovered, and achieve the effect of good curative effect and great development prospect.
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Embodiment 1
[0016] Embodiment 1: Preparation of Magnolia officinalis ethanol extract
[0017] Percolation method: take 5000g magnolia officinalis dried skin powder and percolate with 6 times the amount of 95% ethanol, and the percolation speed is 15ml / min. Recover the ethanol leachate, recover the ethanol under reduced pressure until there is no ethanol smell, concentrate to obtain the extract, and set aside.
[0018] Generally, the ethanol concentration used here can be any value between 75% and 95%. The ethanol used in this embodiment can also be replaced by various alcohols such as methanol and propanol; other organic solvents such as ethyl acetate and ether solvents can also be used. replace
Embodiment 2
[0019] Embodiment 2: Magnolia officinalis supercritical extract preparation supercritical extraction: Magnolia officinalis 200g is pulverized into coarse powder (crossing 40 mesh sieves), puts 1L supercritical CO 2 In the extraction kettle, adjust the pressure: 25MPa, temperature: 45°C, flow rate: 30kg / h, extraction time: 2h. Collect the extracts.
Embodiment 3
[0020] Example 3: Determination of the efficacy of Magnolia officinalis on tumor stem cells
[0021] Experimental method: peripheral blood or bone marrow cells of patients with acute myeloid leukemia and blast criss chronic myeloid leukemia. Peripheral blood cells use leukocyte separation medium to remove red blood cells, and bone marrow cells use 150mM NH 4 Cl and 10 mM NaHCO 3 Red blood cells were removed by treatment for 5 minutes. The cells were washed three times with serum-free medium, and the ethanol extract of Magnolia officinalis obtained in Example 1 (final concentration was 0, 5, 10 μg / ml) was added to treat for 4 hours, or cytarabine was added (final concentration was 0, 5, 10 μg / ml). Then wash three times with serum-free medium to remove Magnolia officinalis ethanol extract, and use methylcellulose IMDM culture fluid (1% methylcellulose, 30% bovine serum albumin, 0.2mM mercaptoethanol, 2mM glutamine , 50ng / ml recombinant human stem cell factor, 10 / ml recombina...
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