Nano-level ultra-high heat-conducting titanium-carbon composite material and preparation method thereof
A composite material and a manufacturing method technology, which are applied in the field of nano-scale ultra-high thermal conductivity titanium-carbon composite material and its manufacturing field, can solve the problems of high price of diamonds and difficult to obtain, and achieve low production cost, enhanced physical structure strength, and simple process. Effect
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Embodiment 1
[0014] Weigh 60Kg of acidified expanded graphite with a carbon content of 90%, 20Kg of flake graphite nanopowder with a carbon content of 90%, 10Kg of titanium metal nanopowder and 10Kg of mesophase nanocarbon powder, and gradually put them into a high-temperature reaction furnace. Under the protection of gas, the temperature is gradually increased from 350°C to 500°C and mixed for 3 hours to obtain a thick high-temperature mixed carbon-making mixed liquid, and then the thick high-temperature mixed carbon-made mixed liquid is hot-molded, and the molding temperature is 450°C. The pressure is 300MPa and molded into a sheet, and finally the molded material is carbonized at 1000°C for 1 hour, and then graphitized at 3000°C for 1 hour. The resulting material has a thermal conductivity of 517W / mK and a density of 1.81g / cm 3 .
Embodiment 2
[0016] Weigh 65Kg of acidified expanded graphite with a carbon content of 92%, 10Kg of flake graphite nanopowder with a carbon content of 91%, 15Kg of titanium metal nanopowder and 10Kg of mesophase nanocarbon powder, and gradually put them into a high-temperature reaction furnace under the protection of an inert gas Gradually increase the temperature and mix at a temperature of 300°C-500°C for 2 hours to obtain a thick high-temperature mixed carbon-making mixed liquid. Then the thick carbon mixed liquid is rolled into a sheet at a rolling temperature of 400°C and a pressure of 180 MPa. Finally, the rolled material is carbonized at 900°C for 4 hours and graphitized at 2500°C for 4 hours. The resulting material has a thermal conductivity of 563W / mK and a density of 1.89g / cm 3 .
Embodiment 3
[0018] Weigh 70Kg of acidified expanded graphite with a carbon content of 90%, 15Kg of flake graphite nanopowder with a carbon content of 90%, 7Kg of titanium metal nanopowder and 8Kg of mesophase nanocarbon powder, and gradually put them into a high-temperature reaction furnace under the protection of an inert gas. Gradually heat up and mix at a temperature of 350°C-450°C for 3 hours to obtain a thick high-temperature mixed carbon-making mixed liquid, and then hot-mold the thick high-temperature mixed carbon-making mixed liquid at a molding temperature of 325°C and a pressure of 230MPa. Formed into sheets, and finally the molded material was carbonized at 920°C for 6 hours, and graphitized at 2900°C for 6 hours. The resulting material has a thermal conductivity of 610W / mK and a density of 1.93g / cm 3 .
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Abstract
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