Protective adhesive film, screen panel and mobile electronic terminal
A technology of adhesive film and adhesive layer, applied in the direction of electronic equipment, adhesive, adhesive type, etc., can solve the problems of foaming, surface hardness reduction, insufficient surface hardness of adhesive sheet, etc., to achieve suitable bonding force, the effect of alleviating the sag of the film, and realizing the adhesive force
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[0164] Hereinafter, the present invention will be described more specifically by way of examples and comparative examples, but the present invention is not limited to these examples.
Synthetic example 1
[0166]
[0167] Add 250 mass parts glycidyl methacrylate (hereinafter referred to as GMA), 1.6 mass parts lauryl mercaptan, 1000 mass parts methyl isobutyl ketone ( Hereinafter referred to as MIBK) and 7.5 parts by mass of 2,2'-azobisisobutyronitrile (hereinafter referred to as AIBN), the temperature was raised to 90° C. over 1 hour while stirring under a nitrogen stream, and the mixture was reacted at 90° C. for 1 hour. Next, a mixed liquid consisting of 750 parts by mass of GMA, 4.4 parts by mass of lauryl mercaptan, and 22.5 parts by mass of AIBN was added dropwise over 2 hours while stirring at 90° C., and then reacted at 100° C. for 3 hours. Subsequently, 10 parts by mass of AIBN was added and reacted at 100° C. for 1 hour, then the temperature was raised to about 120° C. and reacted for 2 hours. Cool to 60°C, replace the nitrogen inlet tube with an air inlet tube, add 507 parts by mass of acrylic acid (hereinafter referred to as AA), 2 parts by mass of p-methoxyphenol,...
Synthetic example 2
[0169]
[0170]Add 200 parts by mass of GMA, 50 parts by mass of n-butyl methacrylate (hereinafter referred to as nBMA), 1.8 parts by mass of lauryl mercaptan, 1000 parts by mass of MIBK and 7.5 parts by mass of AIBN were heated up to 90° C. over 1 hour while stirring under a nitrogen flow, and reacted at 90° C. for 1 hour. Next, a mixed liquid consisting of 600 parts by mass of GMA, 150 parts by mass of nBMA, 4.8 parts by mass of lauryl mercaptan, and 22.5 parts by mass of AIBN was added dropwise over 2 hours while stirring at 90°C, and reacted at 100°C for 3 hours. Subsequently, 10 parts by mass of AIBN was added and reacted at 100° C. for 1 hour, then the temperature was raised to about 120° C. and reacted for 2 hours. Cool to 60°C, replace the nitrogen inlet tube with an air inlet tube, add 406 parts by mass of AA, 2 parts by mass of p-methoxyphenol, and 5.4 parts by mass of triphenylphosphine and mix them, and bubble the reaction solution with air. The temperature was ...
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