475 results about "Dynamic viscoelasticity" patented technology

A film adhesive for sealing a plurality of chip-type devices on a substrate at one time, including an adhesive layer of an adhesive composition which exhibits a minimum value of a storage modulus of elasticity before curing from 1x10<3 >to 5x10<5 >Pa measured by using a dynamic visco-elasticity measuring apparatus while elevating the temperature from 80° C. to 150° C. at an elevating temperature rate of 2.4° C. / min and at a shearing rate of 6.28 rad / sec and a storage modulus of elasticity after curing from 5x10<5 >to 5x10<7 >Pa measured by using a dynamic visco-elasticity measuring apparatus at a sample temperature of 150° C. in a tensile mode at a measuring frequency of 6.28 rad / sec.

The invention provides a sulfur vulcanizable silica-reinforced elastomeric compound having improved tensile mechanical and dynamic viscoelastic properties. The compounds are formed by mixing an elastomer optionally having an alkoxysilane terminal group, with silica in the presence of an alkyl alkoxysilane and a blocked mercaptosilane. In particular, the mercaptosilane moiety of the blocked mercaptosilane and the alkyl alkoxysilane are present in a weight ratio of about 0.001:1 to about 0.20:1. Preferably, the blocked mercaptosilane and the alkyl alkoxysilane are compounded with the elastomer and the silica at high temperature to facilitate the silica-silane reaction. A deblocking agent is added at any desired mixing stage, optionally with the cure package, to allow binding of the mercaptosilane to the polymer.

A retroreflective sheet comprises a film having a substantially flat surface and a large number of pyramidal projections having retroreflectivity on the opposite surface, and a colored layer and an adhesive layer disposed on the surface of the film having the projections. The adhesive layer comprises a heat-sensitive adhesive containing an acrylic polymer and a phenolic resin, and exhibits an elastic modulus (by dynamic viscoelasticity measurement, compression mode) at 30 DEG C. ranging from about 1x106 to 1x108 dyn / cm2.

The present invention provides a biaxially oriented film of a polylactic acid resin that is suitable for films for bags and packaging films for various windows, particularly films for outlook window envelopes. The film is biodegradable and, as films for outlook window envelopes, is superior in the coating adaptability for an antistatic agent, a lubricant and an antiblocking agent or the like and in the high-speed cutting property.The present invention discloses a biaxially oriented film of a polylactic acid resin comprising not less than 50% by weight of a polylactic acid resin, which has a storage modulus E′at 80° C. within the range from 10 MPa to 3,000 MPa, as determined by the test method for temperature dependency of dynamic viscoelasticity, in accordance with JIS K7198 (method A); a heat shrinkage of not higher than 10%, upon heating at 80° C. for 10 seconds; and a tear strength in the width direction (TD direction) of the film of 10 to 200 mN, as determined in accordance with JIS K7128 (method B).

The invention provides an interlayer film for a laminated glass and a laminated glass,which are protected against a slump in TL value through attenuation of said coincidence effect and adapted to display an outstanding sound insulation performance over a broad temperature range.An interlayer film for a laminated glass comprising a plasticizer and a polyacetal resin,which is a blend of a polyacetal resin having an average polymerization degree of 1,000 to 3,000 and a polyacetal resin having an average polymerization degree of 3,000 to 5,000, andwhich has an acetalization degree of 60 to 85 mol % and an acetyl group content of 8 to 30 mol %.An interlayer film for a laminated glasswhich shows a temperature dependence of loss tangentin which the lowest-temperature side maximum of loss tangent appears at 30° C. or lower when examined for dynamic viscoelasticity.

The invention relates to a preparation method of cross-linking hyaluronic acid microgel for tissue filler; wherein, the monolithic gel is generated by the cross-linking reaction of the hyaluronic acid and the di-epoxide in the certain mold and processed by acid solution; the purification and dialysis by physiological balanced solution are processed; the microgel is made by extrusion of mechanical equipment. The cross-linking hyaluronic acid microgel has the advantages of (1) specific physical properties that the storage modulus (G') is 500-2000Pa, the loss modulus (G'') is 50-200Pa, the phase angle (Delta) is below 20 and the complex viscosity (Eta*) is 10-3500Pa x s as described by the dynamic viscoelasticity at frequency of 0.05-10Hz, (2) good stability that the performance of gel is independent of high pressure-high temperature treatment and the enzymolysis-resistant performance is excellent, (3) injectable property that the size of fine particle is 50-1000Mum, (4) good biocompatibility of no cytotoxicity, (5) biodegradability of being fully degraded by hyaluronidase, and (6) being suitable for tissue filler and bio-medical treatment.

Disclosed is a topical composition comprising: (1) a porous spherical disintegrative silica impregnated with a water-insoluble skin benefit agent, wherein: (a) the porous spherical disintegrative silica has an average volume particle size of from about 3 μm to about 20 μm, a maximum particle size of no more than about 50 μm, and a pore volume of from about 1.5 cm3 / g to about 3.0 cm3 / g; and provides a certain dynamic viscoelasticity when sheared; (b) the water-insoluble skin benefit agent having a solubility in water at less than about 0.1 g / l at 25° C. and having a molecular weight of no more than about 5,000, selected from the group consisting of liquid water-insoluble skin benefit agents, solid water-insoluble skin benefit agents which dissolve in liquid water-insoluble skin benefit agents, solid water-insoluble skin benefit agents which dissolve in emollients and / or volatile solvents, and mixtures thereof; and (2) a suitable carrier.

The present invention provides an outer sole light in weight and excellent in abrasion resistance.The outer sole of the present invention is formed out of a polymer composition with a specific gravity of 0.95 or less, which contains an olefin resin and a styrene elastomer, wherein a storage elastic modulus [E′] and a loss coefficient [tan δ] in a dynamic viscoelasticity measurement (20±3° C., 10 Hz) are 100 MPa to 500 MPa and 0.2 or less respectively, and a maximum tensile stress is 30 MPa or more. The olefin resin contains an ethylene polymer and a propylene polymer, for example. The styrene elastomer contains an α-methyl styrene.butadiene copolymer, for example.A flaw is hardly occurred on the outer sole in use, so that the outer sole is excellent in abrasion resistance.

It is to provide a block copolymer and its copolymer composition which provides a heat shrinkable (multilayer) film with less spontaneous shrinkage while maintaining favorable low temperature shrinkability, and a heat shrinkable (multilayer) film containing the block copolymer. By using a block copolymer comprising a vinyl aromatic hydrocarbon and a conjugated diene characterized in that the relation of the loss tangent value obtained by dynamic viscoelasticity measurement with the temperature satisfies specific conditions, or a composition containing the copolymer composition as an essential component, a heat shrinkable (multilayer) film with less spontaneous shrinkability and less odor while maintaining favorable low temperature shrinkability can be obtained.

The present invention provides an optical-use pressure-sensitive adhesive sheet including a pressure-sensitive adhesive layer having, as measured through dynamic viscoelastometry, a storage elastic modulus at 80° C. of at least 2.0×104 Pa and a loss elastic modulus at 80° C. of at least 1.0×104 Pa, in which the pressure-sensitive adhesive sheet has a peel force, as measured in the L-shape peel test, of at least 0.16 MPa, and has a peel distance, as measured in the constant-load peel test (under a load of 100 gf for 3 hours), of at most 50 mm.

A hydrogenated copolymer obtained by hydrogenating an unhydrogenated copolymer comprising conjugated diene monomer units and vinyl aromatic monomer units, the hydrogenated copolymer containing at least one hydrogenated copolymer block (B) which is obtained by hydrogenating an unhydrogenated random copolymer block comprised of conjugated diene monomer units and vinyl aromatic monomer units, wherein the hydrogenated copolymer has the following characteristics: the hydrogenated copolymer has a content of the vinyl aromatic monomer units of from more than 40% by weight to less than 95% by weight; at least one peak of loss tangent (tan 8) is observed at −10 to 80° C. in a dynamic viscoelastic spectrum obtained with respect to the hydrogenated copolymer; and substantially no crystallization peak ascribed to the copolymer block (B) is observed at −20 to 80° C. in a differential scanning calorimetry (DSC) chart obtained with respect to the hydrogenated copolymer.

The present invention provides a golf ball comprising a golf ball body and a paint film formed on a surface of the golf ball body, wherein the paint film has a storage modulus (E′) in a temperature range from 120° C. to 150° C. measured under the specific measurement conditions using a dynamic viscoelasticity measuring apparatus of 1.00×107 dyn / cm2 or more and 1.00×108 dyn / cm2 or less and a loss tangent (tan δ) at the temperature of 10° C. of 0.050 or more.

The invention provides a toner that is capable of low-temperature fixing even in high-speed electrophotographic processes while keeping the cleaning performance when used at high temperatures and the high-temperature storage stability. This toner having toner particles, each of which contains a binder resin and a colorant is characterized in that the temperature of Tp [° C.] when the loss elastic modulus obtained by dynamic viscoelastic measurements on the toner exhibits a maximum value in the temperature range from at least 30° C. to not more than 200° C., is from at least 40° C. to not more than 55° C., and in that, with G″(Tp) [Pa] being this maximum value, G″(Tp+15) [Pa] being the loss elastic modulus at the temperature of Tp+15 [° C.], and G″(Tp+30) [Pa] being the loss elastic modulus at the temperature of Tp+30 [° C.], G″(Tp), G″(Tp+15), and G″(Tp+30) satisfy prescribed relationships.

A vulcanizable rubber composition is presented that comprises an elastomer; a reinforcing filler selected from silica, carbon black, and mixtures thereof, a cure agent; and an amino alkoxy-modified silsesquioxane (AMS) comprising one or more compounds selected from the group consisting of an amino AMS, an amino / mercaptan co-AMS, an amino / blocked mercaptan co-AMS, mixtures thereof, and weak acid-neutralized solid and aqueous solutions thereof. Addition of such compounds to the rubber composition provides improved dynamic viscoelastic and mechanical properties of the vulcanized rubber compound and predict that tire components, especially tread stocks, will provide tires having improved snow traction, lower rolling resistance but equal wet traction, increased rebound, decreased hysteresis, and a general improvement in tire performance.

An electrostatic latent image developing toner including, as a binder resin, a crystalline resin and at least one kind of non-crystalline resin, wherein, in a dynamic viscoelasticity measurement by a sine wave vibration method, a minimum value of the relaxation elasticity H in a relaxation spectrum obtained from frequency dispersion characteristics measured at temperatures of 60 and 80 degrees centigrade with a measurement frequency set in the range of 0.1 to 100 rad / sec and measurement strain set in the range of 0.02 to 4.5% is in the range of 10 to 900 Pa / cm2, and a relaxation time λ corresponding to the minimum value is in the range of 1 to 10,000 sec.

A pneumatic radial tire is provided which comprises an under-belt pad (3) provided circumferentially between edge portions of a belt (1) and a carcass in a shoulder portion thereof, the under-belt pad (3) being of a rubber compound containing 10 to 60 parts by weight of carbon black and 3 to 30 parts by weight of silica with a total amount of carbon black and silica being 20 to 65 parts by weight, 2 to 5 parts by weight of sulfur and 0.5 to 3 parts by weight of resorcin or a resorcin derivative all relative to 100 parts by weight of rubber, and 0.5 to 2 parts by weight of hexamethylene tetratine or a melamine derivative as a methylene donor relative to 1 part by weight of the resorcin or the resorcin derivative, and having a dynamic viscoelasticity E' of 5 MPa to 10 MPa, a loss tangent tan delta of 0.10 to 0.18 and a 300% modulus of 11 MPa to 15 MPa.

The present invention provides a double-sided pressure-sensitive adhesive sheet, including at least one pressure-sensitive adhesive layer which has a gel fraction of 10 to 70%, has a storage modulus at 23 DEG C. of 1105 Pa or less, and has a residual stress after 180 seconds of 3.5 N / cm2 or less, the storage modulus at 23 DEG C. being measured in accordance with a dynamic viscoelasticity measurement and the residual stress after 180 seconds being measured in accordance with a tensile stress relaxation test under conditions of a temperature of 23 DEG C. and a strain of 300%.

This invention provides a multilayer coating film-forming method which comprises applying a first clear paint onto a coating object, applying onto so formed first clear coating film which is either uncured or cured by heating, a second clear paint such that its heat-cured film thickness falls within a range of 2-15 μm, and forming the second clear coating film, (a) the first clear paint and second clear paint comprising hydroxyl-containing resin as the base resin and polyisocyanate compound as the crosslinking agent, and (b) when the coating film formed by applying a paint to a cured film thickness of 40 μm and curing it by heating at 140° C. for 30 minutes is measured of its dynamic viscoelasticity at a frequency of 11 Hz, the first clear paint forming the first clear coating film having a glass transition temperature of lower than 70° C. and tan δ (=loss elastic modulus / storage elastic modulus) at 80° C. of less than 0.4, and the second clear paint forming the second clear coating film having a glass transition temperature of at least 70° C.

The present invention provides a toner for developing an electrostatic latent image comprising at least a core layer including at least a coloring agent and a first binder resin, and a shell layer for covering the core layer and including a second binder resin, wherein two local maximum values of the tangent loss (tan δ) of the dynamic visco-elasticity are present in a temperature range of 90° C. or less, with one of the local maximum values present in a range of less than 60° C., and the other local maximum value present in a range of 60° C. or more and 90° C. or less. Moreover, a production method for the toner for developing an electrostatic latent image, a developer for developing an electrostatic latent image, using the toner, and an image forming method are provided.

The invention provides vulcanizable rubber compound having improved tensile mechanical and dynamic viscoelastic properties. The compounds are formed by mixing an elastomer, containing unsaturated carbon-carbon bonds in its molecular structure, with a reinforcing inorganic filler silica in the presence of an alkyl alkoxysilane and a non-sulfur coupling agent that binds to the rubber backbone with an “ene” linkage or a 1,3 dipolar addition linkage. In particular, the coupling agent and the alkyl alkoxysilane are present in the compound in a weight ratio of about 0.0001:1 to about 1:1.

An asphalt composition comprising from 0.5 to 50 parts by weight of a hydrogenated conjugated diene copolymer (a) and 100 parts by weight of asphalt (b), wherein the hydrogenated conjugated diene copolymer (a) comprises a polymer block (A) comprising vinyl aromatic monomer units and at least one hydrogenated copolymer block (B) obtained by hydrogenation of a non-hydrogenated random copolymer block comprising conjugated diene monomer units and vinyl aromatic monomer units, the hydrogenated conjugated diene copolymer (a) having the following characteristics (1) to (5): (1) the content of the vinyl aromatic monomer units is more than 30% and not more than 60% by weight per weight of the hydrogenated conjugated diene copolymer; (2) the content of the polymer block (A) is from 5% to 50% by weight per weight of the hydrogenated copolymer; (3) the weight average molecular weight is from 30,000 to 500,000; (4) the percentage of hydrogenation of the double bonds in the conjugated diene monomer units is from 60% to 100%; and (5) at least one peak of the loss tangent (tan δ) is present in the range of from −40° C. to less than −10° C. in a dynamic viscoelastic spectrum obtained with respect to the hydrogenated copolymer.

Improvements in the tensile mechanical properties and dynamic viscoelastic properties of silica-reinforced sulfur-vulcanized rubbers can be achieved by compounding elastomers with silica, in the presence of a silane and a catalytic amount of an alkyl tin compound at a high compounding temperature.

A surface protecting adhesive film for a semiconductor wafer in which an adhesive layer is formed on one surface of a base film, wherein the adhesive layer comprises 100 weight parts of a polymer (A) having a functional group capable of reacting with a cross-linking agent and a temperature in a range of from −50° C. to 5° C. at which tan δ of a dynamic viscoelasticity is maximized, from 10 weight parts to 100 weight parts of a polymer (B) having a functional group capable of reacting with a cross-linking agent and a temperature in a range of from more than 5° C. to 50° C. at which tan δ of a dynamic viscoelasticity is maximized, and from 0.1 weight part to 10 weight parts of a cross-linking agent (C) having more than 2 cross-linking reactive functional groups in a molecule based on 100 weight parts of total amount of the polymers (A) and (B), and the surface protecting adhesive film for a semiconductor wafer which the thickness of the adhesive layer is from 5 μm to 50 μm has an excellent adhesion, prevention of breakage and contamination resistance.

The present invention provides an interlayer film for laminated glass which has excellent sound insulating properties even when the thickness is reduced, and also hardly causes optical unevenness.An interlayer film for laminated glass includes at least one layer A containing a thermoplastic elastomer, wherein the shear storage modulus of the layer A at 70° C. as measured by performing a dynamic viscoelasticity test at a frequency of 1,000 Hz in accordance with ASTM D4065-06 is 1 MPa or more, and a layer having a higher shear storage modulus than the layer A is provided on at least one surface of the layer A, and at least one surface of the interlayer film for laminated glass is in a state of having been shaped.

The present invention provides a polyvinyl acetal resin composition exerting excellent mechanical strength over a wide temperature range from low temperatures to high temperatures. The present invention provides a polyvinyl acetal resin composition containing a polyvinyl acetal resin and a resin having a crosslinked structure, the polyvinyl acetal resin composition having a structure in which the resin having a crosslinked structure is dispersed as a dispersed phase in the polyvinyl acetal resin as a continuous phase, the polyvinyl acetal resin composition having a maximum value of a loss tangent derived from the polyvinyl acetal resin at 40° C. or higher and a maximum value of a loss tangent derived from the resin having a crosslinked structure at 10° C. or lower in measurement of a dynamic viscoelasticity spectrum at a frequency of 10 Hz.

The present invention provides a double-sided pressure-sensitive adhesive sheet, including at least one pressure-sensitive adhesive layer which has a gel fraction of 10 to 70%, has a storage modulus at 23° C. of 1×105 Pa or less, and has a residual stress after 180 seconds of 3.5 N / cm2 or less, the storage modulus at 23° C. being measured in accordance with a dynamic viscoelasticity measurement and the residual stress after 180 seconds being measured in accordance with a tensile stress relaxation test under conditions of a temperature of 23° C. and a strain of 300%.

The present invention provides an optical pressure-sensitive adhesive sheet in which white turbidity is not caused by humidification and durability is excellent as well. The present invention provides an optical pressure-sensitive adhesive sheet, comprising: a pressure-sensitive adhesive layer in which a moisture ratio after storage under an environment of 60° C. and 95% RH for 120 hours is 0.65 wt % or more, and a shear storage elastic modulus at 85° C. which is measured by a dynamic viscoelastic measurement is 5.0×104 to 5.0×105 Pa, wherein a peeling distance measured by the constant-load peel test is 30 mm or less when an adherend is a polyethylene terephthalate plate, and the peeling distance measured by the following constant-load peel test is 30 mm or less when the adherend is an acrylic plate.

The invention provides a transmission belt that can suppress lowering in transmission efficiency and has improved durability. A rubber layer adhered to core wires is formed to have a durometer hardness (shore A) of not less than 72 and not more than 85, or have a tensile stress of not less than 0.5 MPa and not more than 1.7 MPa when stretched 10% in the belt longitudinal direction at 25° C., and the rubber layer is formed to have a weight increase of 90% or less after immersed in light oil for 48 hours at 25° C. or have a weight increase of 80% or less after immersed in toluene for 48 hours at 25° C. Alternatively, the rubber layer adhered to the core wires is formed to have a storage modulus of not less than 10 MPa and not more than 50 MPa and a tan δ of not more than 0.15 as measured by dynamic viscoelasticity measurement under conditions at a static load of 3 kgf / cm2, a dynamic strain of 0.4%, a frequency of 10 Hz and a temperature of 25° C. in a tensile mode in a belt longitudinal direction.

A heat shrinkable film and a heat shrinkable multilayer film excellent in balance of heat resistance, high shrinkability, high shrinkability particularly at a low temperature, resistance to spontaneous shrinkage, chemical resistance and rigidity, are provided. A heat shrinkable film and a heat shrinkable multilayer film obtained from a resin composition comprising an aromatic vinyl compound / conjugated diene block copolymer having a micro phase separation structure comprising a soft phase and a hard phase and further having a specific structure and a specific dynamic viscoelasticity spectrum and a styrene polymer having a syndyotactic structure, in a specific proportion.