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Simulation moving bed reactor and using method thereof

A technology for simulating moving beds and reactors, applied in chemical instruments and methods, chemical/physical processes, etc., can solve the problems of very demanding catalyst mechanical strength, catalyst particle wear, and large equipment, achieving low processing costs, avoiding mechanical Moving, simple structure effects

Inactive Publication Date: 2010-12-15
SHANXI INST OF COAL CHEM CHINESE ACAD OF SCI
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0007] The common problem of the moving bed reactors provided by the above patents is that the catalyst particles need to physically move mechanically in the equipment, resulting in severe wear of the catalyst particles, so the requirements for the mechanical strength of the catalyst are very strict
However, the technology provided by this patent requires the arrangement of multiple fixed-bed reactors, making the device huge and increasing the investment

Method used

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  • Simulation moving bed reactor and using method thereof
  • Simulation moving bed reactor and using method thereof
  • Simulation moving bed reactor and using method thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0035] There are 5, 6, 7 raw material inlets and 8, 9, 10, 11 reaction product outlets on the side wall of the reactor shell 17, and the reaction product outlet ratio on the side wall of the reactor shell 17 is located on the side wall of the reactor shell 17 The import of raw materials is one more. The position of the first raw material inlet 5 on the side wall of the reactor shell 17 is higher than the position of the first reaction product outlet 8 on the side wall of the reactor shell 17, and the second on the side wall of the reactor shell 17 The position of the raw material inlet 6 is higher than the position of the second reaction product outlet 9 on the side wall of the reactor housing 17, and the position of the third raw material inlet 7 on the side wall of the reactor housing 17 is higher than that of the second reaction product outlet 9 located on the side wall of the reactor housing. The position of the third reaction product outlet 10 on the side wall of 17 has a...

Embodiment 2

[0054] The valve of the material inlet 18 at the bottom of the reactor shell 17 is always in an open state, and other conditions and operation methods are exactly the same as those in Example 1.

[0055] Take part of the reaction product at a lower temperature after heat exchange and cooling as the low-temperature material, and enter the reactor shell 17 by making the material inlet 18 at the bottom of the reactor shell 17 flow in the direction opposite to the main reaction material flow direction, And leave the reactor from the same outlet as the main reaction product.

[0056] The reaction conditions and reaction results of the present embodiment are as follows:

[0057] Methanol weight space velocity: 1.0h -1

[0058] (relative to the catalyst between each pair of import and export)

[0059] Cycle ratio: 6

[0060] Reaction material inlet temperature: 380°C

[0061] Reaction material outlet temperature: 440°C

[0062] Reaction pressure: 0.5MPa

[0063] Material space...

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Abstract

One to 30 raw material inlets are arranged on the side wall of a reactor body (17) of a simulated moving bed reactor. The top part of the reactor body (17) is provided with one raw material inlet (2); the bottom part of the reactor body (17) is provided with a material inlet (18). Two to thirty one reaction product outlets are arranged on the side wall of the reactor body (17); the number of the total raw material inlets of the reactor body (17) is equal to that of the reaction product outlets on the side wall of the reactor body (17); the position of the first raw material inlet (5) on the side wall of the reactor body(17) is higher than the position of the first reaction product outlet (8) on the side wall of the reactor body (17); the second material inlet (6) on the side wall of the reactor body(17) is higher than the position of the second reaction product outlet (9) on the side wall of the reactor body (17), and so on. Through switching the valves of the inlets and the outlets, the invention realizes the substantial moving of a catalyst bed and has stable and reliable operation; the service life of the catalyst is effectively prolonged under the situation of not changing theself performance of the catalyst.

Description

technical field [0001] The invention belongs to a reactor used in chemical process and its application method, in particular to a simulated moving bed reactor and its application method. Background of the invention [0002] Most chemical processes involve catalytic reactions. Depending on the life of the catalyst used, the reactor can be in the form of a fixed bed, a moving bed or a fluidized bed. Generally speaking, fixed-bed reactors are often used when the catalyst life is long, such as the methanol synthesis process and the ammonia synthesis process. Complicated process operation, catalyst replacement is infrequent. For the catalyst life of several days or tens of days, moving bed reactors can be used in industry, such as gasoline aromatization modification reaction, ethylene and butene deproportionation to propylene process, the life of the molecular sieve catalyst used is average For tens of days, when a fixed bed reactor is used, the catalyst regeneration is frequen...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): B01J8/02
Inventor 李文怀胡津仙张侃张建利方勇王俊杰邓惠平范伟强孙晓芳章斌田艳青宋国平
Owner SHANXI INST OF COAL CHEM CHINESE ACAD OF SCI
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