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Method for preparing high purity cardanol

A cardanol, high-purity technology, applied in the chemical field, can solve the problems of low yield and low product purity, achieve low viscosity, improve yield and purity, and prevent self-polymerization

Inactive Publication Date: 2008-12-10
上海美东生物材料股份有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] The object of the present invention is to provide a kind of preparation method of high-purity cardanol, the preparation method of described this high-purity cardanol will solve the low yield and product purity in the technology of adopting high-temperature rectification to prepare cardanol in the prior art. low technical issues

Method used

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Embodiment Construction

[0010] A high-purity cardanol preparation method of the present invention includes a process of extracting cardanol from natural cashew nut shell liquid by using a molecular still, wherein the molecular still consists of a cylindrical cylinder, a rotor and a built-in condenser Composition, the cylindrical shell is set in a fixed frame, the built-in condenser is set in the center of the cylindrical shell, the rotor is set on the fixed frame, the lower part of the cylindrical shell A heating device is provided, and a film wiper and an anti-splash device are provided on the fixed frame. During the process of extracting cardanol from the raw material liquid, the natural cashew nut shell liquid is added from the top of the cylindrical cylinder, and at the same time, the Rotate the rotor between the cylinder and the condenser, use the rotor to continuously and evenly distribute the natural cashew nut shell liquid on the heating surface of the cylindrical cylinder, and then use the sc...

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Abstract

The invention discloses a method for preparing a high-purity cardanol. The method comprises a process of extracting a cardanol from a natural cashew nut shell liquid with a molecular still, wherein the molecular still consists of a cylindrical shell, a rotor and a built-in condenser, the lower part of the cylindrical shell is provided with a heater, a fixed frame is provided with a film blade and an antispray device; the natural cashew nut shell liquid is poured into the cylindrical shell from the top and the rotor is rotated between the cylindrical shell and the condenser at the same time to distribute the natural cashew nut shell liquid on a heating surface of the cylindrical shell continuously and evenly; and the film blade is used to spread the feed liquid to a layer of turbostratic liquid film and the film blade is used to spirally push the turbostratic liquid film to the built-in condenser to cool the turbostratic liquid film into a liquid; finally the liquid flows down along a pipe of the condenser and is discharged from a discharge pipe to obtain the high-purity cardanol. The method can improve the yield and purity of the cardanol.

Description

Technical field: [0001] The invention relates to the field of chemistry, in particular to a method for preparing organic polymer compounds, in particular to a method for preparing high-purity cardanol Background technique: [0002] One of the greatest utilization values ​​of petroleum is fine chemical polymer materials, and one of the highest values ​​of biomaterial energy is the effective replacement of fine chemical polymer materials. Studies have shown that cardanol is the most promising non-grain oil substitute among similar biomass chemical materials. Special functional polymer chemical materials can be synthesized with cardanol, which can solve problems that cannot be solved by petroleum phenolic compounds. However, due to technical reasons, the refining and extraction of cardanol has become a major problem, the industrial production of high-purity cardanol cannot be realized, and the utilization value of cardanol is greatly limited. At present, the high-temperature r...

Claims

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Application Information

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IPC IPC(8): C07C39/19C07C37/74C07C37/68
Inventor 黎明
Owner 上海美东生物材料股份有限公司
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