Novel uses of day lily and day lily total flavones
A technology of day lily and total flavonoids, which is applied in the field of new uses and preparations of day lily and total flavonoids of day lily, and can solve problems such as unreported applied research
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Embodiment 1
[0151] Embodiment 1: Capsules
[0152] Cut 9900g of dried day lily into 2-3 cm long sections, soak in 95% ethanol overnight. Heating and extracting with 95% ethanol for 3 times, timing from boiling, the time is 40min, 30min, 30min respectively, filtering, combining the filtrates, recovering ethanol, and obtaining extract A. The residue was heated and extracted twice with 60% ethanol for 40 minutes each time, filtered, the filtrates were combined, and the ethanol was recovered to obtain the extract B. Dilute the extract A with distilled water, filter, pass through the treated AB-8 macroporous resin column, wash with distilled water until the effluent is transparent, elute with 60% ethanol for 3 times the column volume, recover ethanol, and obtain sample 1. Treat extract B in the same way to get sample 2. Sample 1 is 64.3101g, and Sample 2 is 60.9338g. The cream yield is greater than 1.265%. Take the dried extract, add lactose (or starch, or dextrin) at a ratio of 1:0-5, mix ...
Embodiment 2
[0156] Embodiment 2: Preparation and inspection of total flavonoids in day lily
[0157] Cut 9900g of dried day lily into 2-3 cm long sections, soak in 95% ethanol overnight. Heat extraction with 95% ethanol for 3 times, start timing from boiling, the time is 40min, 30min, 30min respectively, filter, combine filtrates, recover ethanol, and obtain extract A. The residue was heated and extracted twice with 60% ethanol for 40 minutes each time, filtered, the filtrates were combined, and the ethanol was recovered to obtain the extract B. Extraction A was diluted with distilled water, filtered, passed through the treated AB-8 macroporous resin column, washed with distilled water until the effluent was transparent, eluted with 60% ethanol for 3 times the column volume, recovered ethanol, and sample 1 was obtained. Treat extract B in the same way to get sample 2. Sample 1 is 64.3101g, and Sample 2 is 60.9338g. The cream yield is greater than 1.265%, and samples 1 and 2 are mixed t...
Embodiment 3
[0163] Embodiment 3: Granules
[0164] Cut 9900g of dried day lily into 2-3 cm long sections, soak in 95% ethanol overnight. Heat extraction with 95% ethanol for 3 times, start timing from boiling, the time is 40min, 30min, 30min respectively, filter, combine filtrates, recover ethanol, and obtain extract A. The residue was heated and extracted twice with 60% ethanol for 40 minutes each time, filtered, the filtrates were combined, and the ethanol was recovered to obtain the extract B. Extraction A was diluted with distilled water, filtered, passed through the treated AB-8 macroporous resin column, washed with distilled water until the effluent was transparent, eluted with 60% ethanol for 3 times the column volume, recovered ethanol, and sample 1 was obtained. Treat extract B in the same way to get sample 2. Sample 1 is 64.3101g, and Sample 2 is 60.9338g. The paste yield is greater than 1.265%. Samples 1 and 2 are mixed, and dextrin is added to make granules through a conven...
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