Silver-containing antimicrobial articles and methods of manufacture
A product, silver salt technology, applied in the field of whitening antibacterial products, manufacturing packaged antibacterial products, can solve the problems of exhaustion, not light stability, leaving stains and so on
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example 1
[0095] Cotton substrate with high anion content coated with silver sulfate
[0096] Silver sulfate (Colonial Metals Inc., Elkton, MD) and water were mixed so that there were 0.1333 grams (g or gm) of AgSO per 100 grams of aqueous solution. 4 , to prepare a silver sulfate coating solution. Spunlace 100% cotton mesh (50g / m 2 ; 30.48 cm wide, manufactured by Spuntech Industries, Upper Tiberius, Israel, and coated with a slot die. The pump speed was 316 mL / min. The coated web was dried at 356°F (180°C). The oven length is 15.24 meters (m). The speed of the web is 3.048m / min. The dried web was golden yellow. It is rolled up and placed in a heat sealable foil pouch. 4.7 mg total silver per gram of dressing (Method: EPA 6010B using ICP-AES). By the method described above, the release of silver ions was determined to be 4.2 milligrams (mg) Ag + / g Dressing.
[0097] The dressings were die cut and placed in various packaging materials at a water activity of 0.5, and the pac...
example 2
[0102] Silver Sulfate Coated Low Anion Cotton Substrate
[0103] The dressing of Example 2 was prepared in the same manner as Example 1, except that the spunlace 100% cotton web was manufactured by Unitika, Osaka, Japan under the trade name COTTOASE, 280 millimeters (mm) wide; 50 Grams per square meter (gm / m 2 ). This resulted in a dressing with a total of 5.5 mg of silver per gram of dressing (Method: EPA6010B using ICP-AES), 3.6 mg of Ag per gram of dressing as measured by the method in the test protocol + release of silver ions. The dried dressing was yellow in color.
[0104] The dressings were die cut and placed in various packaging materials at a water activity of 0.5, and the packages were heat sealed. The packaged silver dressings were electron beam irradiated at 30 kGy or gamma irradiated at 38 kGy. Samples were stored at room temperature for 1 to 8 weeks prior to evaluation for color change. Table 5 presents the results of these evaluations.
[0105] table...
example 3
[0109] Silver Sulfate Coated Low Anion Cotton Substrate
[0110] The dressing of Example 3 was prepared in the same manner as Example 2, except that the drying temperature was 175°F (79°C). Dry silver sulfate coated cotton was white. The dressing has a total amount of 5.3mg Ag per gram of dressing (Method: EPA 6010B using ICP-AES), and as measured by the method in the test protocol, the dressing has 3.5mg Ag per gram of dressing +release of silver ions. Dressings were die cut and placed in various packaging materials at a water activity of 0.5, then activated carbon canister (ACC) liners were added, the packages were heat sealed, and packages with dressings without liners were also prepared. The packaged silver dressings were electron beam irradiated at 30 kGy or gamma irradiated at 38 kGy. Samples were stored at room temperature for 1 to 8 weeks prior to evaluation for color change. The table shows the effect of the presence of activated charcoal in the packaging on the...
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