Medicine composition capable of eliminating the mass and relieving swelling, absorbing clots and alleviating pain, preparation method and quality control method thereof
A technology for removing blood stasis, relieving pain, dispelling stagnation and reducing swelling, applied in drug combinations, medical preparations containing active ingredients, drug delivery, etc.
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experiment example 1
[0039] Experimental Example 1 Process Experimental Research
[0040] 1. Grinding fineness test
[0041] The medicinal materials are configured according to the prescription amount, each serving contains 10g of musk, 90g of wood turtle seed (shelled and deoiled), 90g of Aconitum aconiti, 90g of sweetgum balsam, 40g of frankincense (made), 40g of myrrh (made by), Wulingzhi (made by vinegar) Fried) 90g, Angelica (wine fried) 40g, Dilong 90g, Xiangmo 8g, respectively divided into four groups for experiments: the crushing fineness is: 50 mesh, 65 mesh, 80 mesh, 100 mesh, respectively, according to the pellet viscosity, The appearance of pills and crushing loss are used as indicators to determine the fineness of crushing. The results are shown in Table 1:
[0042] Table 1: Pulverization test results
[0043] Number of groups
[0044] The above results show that: when the crushing fineness is 80 mesh, the indicators are better, so 80 mesh is used in production.
[0045...
experiment example 2
[0053] Experimental example 2 Experimental research on identification method
[0054] 1. Angelica identification test screening
[0055] (1) Preparation of test solution
[0056] Method 1: Take the pharmaceutical preparation of the present invention equivalent to 3.85g of the original medicinal material, grind it finely, add 20ml of ether, ultrasonicate for 10 minutes, filter, evaporate the filtrate to dryness, add 1ml of ethanol to the residue to dissolve, and use it as the test solution.
[0057] Method 2: Take the pharmaceutical preparation of the present invention equivalent to 3.85g of the original medicinal material, grind it finely, add 20ml of ether, ultrasonically treat it for 20 minutes, filter, evaporate the filtrate to dryness, add 1ml of ethanol to the residue to dissolve, and use it as the test solution.
[0058] Method three: take the pharmaceutical preparation of the present invention equivalent to 3.85g of the original medicinal material, grind it finely, add...
experiment example 3
[0109] Experimental example 3 Experimental research on inspection items
[0110] Research on heavy metals and arsenic salts
[0111] 1 heavy metal inspection
[0112] Measuring method: take 2g of the fine powder of this product, put it in a crucible, carbonize at low temperature, and then completely ash at 600°C, add 2ml of hydrochloric acid to the residue, evaporate to dryness in a water bath, add 15ml of water, and check according to the law (Appendix IX E of Chinese Pharmacopoeia 2005 Edition second method). According to the determination method, the heavy metal limit of three batches of samples was checked, and the content was less than 10ppm, so it was not included in the text. The results are shown in Table 1.
[0113] Table 1 Heavy metal inspection results of three batches of samples
[0114] batch number
Heavy metal content in Pb (ppm)
05122101
05122202
05122303
＜10
＜10
＜10
[0115] 2 Arsenic salt inspection
[0116] tes...
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