Extraction method of tuber mustard volatile oil
An extraction method and technology for volatile oil, applied in the field of biochemistry, can solve problems such as hindering in-depth research on volatile oil components, weak extraction method of mustard volatile oil, etc., and achieve the effects of high product yield and low preparation process cost.
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[0021] In this embodiment, volatile oil is extracted from mustard mustard from Chongqing Fuling Mustard Mustard Group as raw material.
[0022] Chop the mustard sample into 4 ~ 8mm 3 The fritter, weighs 100g, is contained in the distillation flask of 1000ml, adds 400ml deionized water, 50 ℃ of insulations, enzymolysis 1 hour, obtain mustard mustard enzymolysis solution.
[0023] Connect the distillation flask containing the enzymatic hydrolysis solution to one end of the simultaneous distillation and extraction device, and control the temperature at 100°C through a heating mantle to maintain a slight boiling state. At the other end, the temperature is controlled at about 40°C by means of water bath heating, and at the same time, distillation and extraction are carried out for 3 hours.
[0024] At the same time, after distillation and extraction are completed, remove the distillation bottle containing ether, add about 8g of anhydrous sodium sulfate to it for dehydration for 15...
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