Shearing cross-linking sensitive plugging agent and preparation method thereof

A technology of sensitivity and plugging agent, which is applied in the field of shear cross-linking sensitive plugging agent and preparation, which can solve the problems of affecting drilling efficiency, affecting drilling speed, poor plugging effect, etc.

Inactive Publication Date: 2009-09-02
JINZHOU HONGLI CHEM TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0002] Lost circulation is a common and serious problem in oilfield drilling, which not only affects the drilling speed, but also causes huge economic losses
At present, the plugging method commonly used at home and abroad is mainly bridge plugging, because it is difficult to accurately judge the properties of the downhole leaking zone (such as the width of the fracture), and the particle size of the plugging agent does not match the width of the crack in the leaking zone, which often leads to poor plugging effect. Repeated loss after Jiahe plugging
At the same time, bridge plugging needs to be tripped during the implementation of plugging, which affects the efficiency of drilling operations

Method used

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Examples

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Effect test

Embodiment Construction

[0018] Below by embodiment the present invention will be further described:

[0019] (1) Preparation of organic titanium kerosene solution

[0020] As a cross-linking agent, organic titanium can link polymer chains containing ~OH to form a body structure. Organic titanium is a titanate compound such as: tetraisopropyl orthotitanate, diisopropyl orthotitanate dilactic acid Any one of ester, bis-triethanolamine diisopropyl orthotitanate, mix organic titanium with kerosene to form organic titanium kerosene solution, the concentration (mass percentage) of organic titanium crosslinking agent in kerosene is 0.1~1.0% .

[0021] (2) preparation of modified guar gum aqueous solution

[0022] Modified guar gum is used as a thickening agent, which is obtained by graft copolymerization of acrylamide, methylolacrylamide monomer and guar gum. The graft copolymerization process is: 0.5-1.5 parts of guar gum Disperse and dissolve, pass nitrogen gas for 1 hour, add 0.001~0.01 parts of ammon...

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Abstract

The invention provides a shearing cross-linking sensitive plugging agent used for the drilling engineering. The plugging agent comprises the following components: 40 to 60 parts of organic titanium coal-oil solution, 40 to 60 parts of modified guar gum solution and 2 to 5 parts of emulsifier, wherein the organic titanium coal-oil solution is the mixture of coal oil and organic titanium, the organic titanium is any one of the titanate compounds, the modified guar gum solution is obtained by the graft copolymerization of acrylamide, hydroxymethyl acrylamide monomer and guar gum, and the emulsifier is fatty acid polyoxyethylene ether. The preparation method comprises the following steps: the 2 to 5 parts of the emulsifier is added to the 40 to 60 parts of the organic titanium coal-oil solution, the emulsifier and the organic titanium coal-oil solution are evenly stirred, then the 40 to 60 parts of the modified guar gum solution is added into the mixture slowly and stirred for 1 hour at the temperature of 30 to 35 DEG C to form stable reversed emulsion through a colloid mill, and the finished product of the shearing cross-linking sensitive plugging agent is further obtained. The shearing cross-linking sensitive plugging agent is used for plugging a drilling, the cross-linking agent can be immediately mixed with macromolecule under the action of the high shearing rate of the bit port to generate cross-linking, and the gelling stemming similar to the plastic solid is formed so as to rapidly block the serious leakage layer.

Description

technical field [0001] The invention relates to the field of drilling plugging engineering, in particular to a shear cross-linking sensitive plugging agent and a preparation method. Background technique [0002] Lost circulation is a common and serious problem in oilfield drilling, which not only affects the drilling speed, but also causes huge economic losses. At present, the plugging method commonly used at home and abroad is mainly bridge plugging, because it is difficult to accurately judge the properties of the leaking layer (such as the width of the fracture) in the downhole, and the particle size of the plugging agent does not match the width of the fracture in the leaking layer, which often leads to poor plugging effect. Repeated leaks occurred after Jiahe plugged the leak. At the same time, bridge plugging needs to be tripped during the implementation of plugging, which affects the efficiency of drilling operations. In recent years, from the research and applicati...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C09K8/42
Inventor 刘莉高丽
Owner JINZHOU HONGLI CHEM TECH
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