Ibuprofen composition
A technology of mixtures and polymers, applied in the directions of microcapsules, capsule delivery, organic active ingredients, etc., can solve the problems of reducing coating, disadvantage, etc.
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Embodiment 1
[0057] Embodiment 1: ibuprofen tablet formula A
[0058] Part A: Preparation of ibuprofen granulation formula A
[0059] First in a Glatt 5 / 9 top-spray fluidized bed granulator, mix ibuprofen, dextrose, citric acid and hydroxypropyl methylcellulose with an air flow rate of 3.6 scfm (standard cubic feet per minute) to form The mixture was granulated, whereby a granulate comprising the ingredients in Table A below was prepared.
[0060] In a laboratory mixer set at a speed of 75 RPM, 90 grams of starch was added to 1497 grams of cold water while stirring to obtain a starch paste solution with 5.67% solids. The solution was heated with stirring until its temperature reached 75°C. The resulting solution was then sprayed into the granulation mixture at a rate of about 50 g / min at a product temperature of about 27°C and an atomization pressure of 1.5 bar before drying to a final product temperature of 32°C. use Computrac TM Max 2000 measured the loss on drying (LOD) value at ...
Embodiment 2
[0085] Embodiment 2: ibuprofen tablet formula B
[0086] Part A: Preparation of Ibuprofen Granules Formula B
[0087] Ibuprofen, dextrose, citric acid and hydroxypropyl methylcellulose were first mixed at an air flow rate of 350 scfm in a 90-liter fluidized bed granulator equipped with an 18-inch Worster column and spray gun to form Formulation mixture, thus prepared granules comprising the ingredients in Table E below.
[0088] Three batches of granulation solution were prepared simultaneously in a 55 gallon stainless steel tank. In preparing each batch of granulation solution, 480 g of starch was added to 7.99 kg of cold water while stirring using an air mixer equipped with low shear blades set at a speed of 50 RPM to obtain a starch paste solution containing 5.67% solids. This solution was heated with stirring until its temperature reached 79°C to obtain a granulation solution. The resulting granulation solution is then sprayed into the granulation mixture at a rate ...
Embodiment 3
[0114] Embodiment 3: ibuprofen tablet formula C
[0115] Part A: Preparation of Tablets for Evaluation - Formulation C
[0116] Preparation of Tablet Blend Base:
[0117] Table I - Tablet Base Blend Formulation C
[0118] Element
Percentage (weight / weight)
mg / tablet
Coated Granulated Ibuprofen *
17.3
241.5
Dextrose monohydrate (coarse grade)
75.4
1055.6
cross-linked polyvinylpyrrolidone
NF **
2.1
29.0
artificial grape flavoring
0.3
4.5
1.07
15.0
0.14
2.0
Fumaric acid NF
1.64
23.0
Citric Acid USP
0.21
3.0
[0119] FD&C Blue L#1 Aluminum Lake
0.10
1.4
D&C red calcium lake
0.07
1.0
1.07
15.0
Sucralose NF
0.64
9.0
total
100.0
14...
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