Method for preparing glycerin zinc
A technology of zinc glycerol and glycerin solution, which is applied in the field of preparation of zinc glycerol, can solve the problems of long reaction time, harsh synthesis conditions, troublesome operation, etc., and achieve the effect of simple and easy synthesis process
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example 1
[0015] Example 1, take 0.005mol / L Zn(CH 3 COO) 2 2H 2 O glycerol solution in a 50mL round-bottomed flask, put the round-bottomed flask into a microwave oven, 680W power, and microwave for 3 minutes. Glycerol zinc nanoparticles with a particle diameter of 23 nm were obtained by centrifugation.
example 2
[0016] Example 2, take 0.006mol / L Zn(CH 3 COO) 2 2H 2 O glycerol solution in a 50mL round-bottomed flask, put the round-bottomed flask into a microwave oven, 740W power, and microwave for 4 minutes. Glycerol zinc nanoparticles with a particle size of 29 nm were obtained by centrifugation.
[0017] Example 3, take 0.007mol / L Zn(CH 3 COO) 2 2H 2 O glycerol solution in a 50mL round-bottomed flask, put the round-bottomed flask into a microwave oven, 800W power, and microwave for 4 minutes. Glycerol zinc nanoparticles with a particle size of 37 nm were obtained by centrifugation.
[0018] Example 4, take 0.008mol / L Zn(CH 3 COO) 2 2H 2 O glycerol solution in a 50mL round-bottom flask, put the round-bottom flask into a microwave oven, 800W power, and microwave for 6 minutes. Glycerol zinc nanoparticles with a particle diameter of 48nm were obtained by centrifugation.
[0019] Example 5, take 0.08mol / L Zn(CH 3 COO) 2 2H 2 O glycerol solution in a 50mL round-bottom flask,...
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