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Method for separating silicon carbide from silicon carbide micro-powder graded byproducts

A technology of silicon carbide micropowder and by-products, which is applied in the field of separating silicon carbide from the by-products of silicon carbide micropowder classification, can solve the problems of waste of manpower, material and financial resources, potential safety hazards of operators, and long processing time, so as to improve work efficiency and improve economic efficiency. Efficiency, the effect of large processing capacity

Inactive Publication Date: 2012-02-22
PINGDINGSHAN YICHENG NEW MATERIAL
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, in the process of carbon washing, a small amount of silicon carbide particles will be washed out together with free carbon to form a by-product carbon material. The market price of carbon material is very low, and it contains a large amount of silicon carbide micropowder particles. would be a huge waste
The traditional method of recovering silicon carbide micropowder contained in carbon materials is still processed by carbon washing process. This method is more suitable for raw materials with low carbon content, and the traditional method has long processing time and requires a large amount of Acidic substances and alkaline substances have a great impact on the environment, and at the same time pose a safety hazard to operators, and waste a lot of manpower, material and financial resources

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0030] The method that the present invention handles the by-product carbon material that contains free carbon content at 90% is: drop into about 1 ton of carbon material in the treatment pool 1, add 3 tons of deionized water, add the lye of 3 ‰ of carbon material weight, lye concentration 30%, adjust the pH value of the solution to 10, leave it to stand and soak for 2 hours, two layers appear in the material in the pool I to be treated, the uppermost layer is a carbon material layer containing 90% carbon, and the lower layer is silicon carbide micropowder containing 1.5% carbon Layer, using siphon extraction or water pump to extract the carbon material in the treatment tank I, the bottom of the treatment tank I is the collected silicon carbide powder; collect the extracted carbon material slurry into the treatment tank II, and add the slurry respectively 0.5‰ of lye and dispersant by weight, the concentration of lye is 30%, the pH value of the solution is adjusted to 10, and it...

Embodiment 2

[0032] The method that the present invention handles the by-product carbon material that contains free carbon content at 85% is: drop into about 0.7 tons of carbon material in the treatment pool 1, add 2.5 tons of deionized water, add the lye of 2.5 ‰ of carbon material weight, lye concentration 60%, adjust the pH value of the solution to 11, let it stand and soak for 4 hours, two layers appear in the material in the pool I to be treated, the uppermost layer is a carbon material layer containing 80% carbon, and the lower layer is a silicon carbide micropowder layer containing 1.2% carbon , use the method of siphon extraction or water pump to extract the carbon material in the treatment tank I, and the material at the bottom of the treatment tank I is the collected silicon carbide powder; collect the extracted carbon material slurry into the treatment tank II, and add the slurry 0.7‰ of lye and dispersant by weight, the concentration of lye is 60%, adjust the pH value of the sol...

Embodiment 3

[0034]The method that the present invention handles the by-product carbon material containing free carbon content at 45% is: drop into about 0.8 tons of carbon material in the treatment pool 1, add 4 tons of deionized water, add the lye of 0.5 ‰ of carbon material weight, the concentration of lye 45%, adjust the pH value of the solution to 7.5, stand and soak for 5 hours, two layers appear in the material in the pool I to be treated, the uppermost layer is a carbon material layer containing 85% carbon, and the lower layer is a silicon carbide micropowder layer containing 1% carbon , use the method of siphon extraction or water pump to extract the carbon material in the treatment tank I, and the material at the bottom of the treatment tank I is the collected silicon carbide powder; collect the extracted carbon material slurry into the treatment tank II, and add the slurry 3‰ of lye and dispersant by weight, the lye concentration is 45%, the pH value of the solution is adjusted t...

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PUM

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Abstract

The invention discloses a method for separating silicon carbide from silicon carbide micro-powder graded byproducts, which comprises the following steps of: filling a carbon material into a treatment pond I, adding deionized water in an amount which is 2 to 5 times the weight of the carbon material and alkali liquor in an amount which is 0.05 to 0.3 of the weight of the raw carbon material into the treatment pond I, and standing the mixture for 2 to 5 hours; after demixing treatment, collecting slurry of a carbon material layer to a treatment pond II, adding alkali liquor and dispersant in anamount which is 0.05 to 0.3 percent of the weight of the slurry respectively into the treatment pond II, and standing the mixture for 3 to 4 hours; and demixing the mixture again to obtain separated silicon carbide micro-powder on the lower layer. Material addition and demixing treatment are performed twice, wherein the secondary treatment is performed under the condition that most carbon is removed in the first time; the added dispersant is used for separating carbon particles adhered to certain silicon carbide particles and separating the silicon carbide particles adhered to the carbon particles, so the treatment effect is promoted, the separated silicon carbide micro-powder has higher purity, and more values are created for enterprises.

Description

technical field [0001] The invention relates to a method for recovering silicon carbide micropowder, in particular to a method for separating silicon carbide from by-products of silicon carbide micropowder classification. Background technique [0002] At present, in the silicon carbide powder classification process, some by-products will be produced, and one of the by-products is called carbon material (we collectively refer to carbon material with a free carbon content greater than 50%), which is carbonized through a unique foaming carbon washing process The separation of free carbon in silicon fine powder from silicon carbide powder is a current processing method at home and abroad. However, in the process of carbon washing, a small amount of silicon carbide particles will be washed out together with free carbon to form a by-product carbon material. The market price of carbon material is very low, and it contains a large amount of silicon carbide micropowder particles. wo...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C01B31/36
Inventor 曲丽伟杨正宏徐大慧
Owner PINGDINGSHAN YICHENG NEW MATERIAL
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