Heavy oil suspension bed hydro-upgrading method
A hydro-upgrading and suspended-bed technology, which is used in hydrocarbon oil cracking, petroleum industry, etc., to reduce operating costs, increase yield, and ensure the effect of hydrogenation.
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Embodiment 1
[0023] A certain amount of molybdenum naphthenate is directly added in the heavy oil raw material, then adopts the mode of magnetic stirring, catalyst is dispersed in the heavy oil raw material (main properties see table 1); Metal weight calculation) aqueous solution of nickel phosphomolybdate, surfactant Tween-85 and co-surfactant n-hexanol are fully mixed and then added to the above-mentioned heavy oil raw material, and the catalyst aqueous solution is uniformly dispersed in the heavy oil by high-shear stirring method In the raw material, the obtained mixed raw material is then mixed with hydrogen into a high-temperature and high-pressure reactor for hydrogenation reaction. After the reaction, the product is distilled under normal pressure to obtain gasoline fraction, diesel fraction and hydrogenated tail oil. The operating conditions and test results are listed in the table. 2 and Table 3.
Embodiment 2~4
[0030] According to the process described in Example 1, using the conditions described in Table 4, the reaction results are shown in Table 5.
[0031] Table 1 Properties of heavy oil raw materials
[0032]
[0033]Table 2 Embodiment 1 and comparative example operating conditions
[0034]
[0035] Table 3 embodiment 1 and comparative example test result
[0036]
[0037] Table 4 Embodiment 2~4 operating conditions
[0038]
[0039] Table 5 Example 2~4 test results
[0040]
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