Preparation method of calamine cellulose fiber
A cellulose fiber, calamine technology, applied in the direction of rayon, single-component cellulose rayon, fiber processing and other directions in cellulose solution, can solve the problem of reducing the content of calamine in the finished fiber and affecting the acid bath. The content of zinc sulfate in the middle, the loss of active ingredients of calamine, etc., can improve the spinnability, improve the functional index, and avoid damage.
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Embodiment 1
[0029] Embodiment 1: the preparation method of calamine cellulose fiber, comprises the following steps:
[0030] (1) calamine slurry preparation process: get the calamine that particle diameter is 125nm, add relative calamine weight and be 0.3% dispersant dialkyl dimethyl ammonium chloride and relative calamine in calamine weight Calamine weight is the dispersant polysiloxane quaternary ammonium salt of 0.5%, adds deionized water again, is configured into the calamine slurry that weight percentage concentration is 25%, puts calamine slurry in ball mill, ball milling 100min to make uniform nano calamine slurry;
[0031] (2) Preparation process of spinning stock solution: pulverize cotton pulp with a degree of polymerization of 330 and then mix it evenly with 1-allyl, 3-methylclomidazolium salt solution, dissolve at 90°C to form a uniform and stable spinning stock solution , the concentration by weight of cellulose in the spinning dope is 5%;
[0032] (3) Preparation process o...
Embodiment 2
[0038] Embodiment 2: the preparation method of calamine cellulose fiber, comprises the following steps:
[0039] (1) calamine slurry preparation process: get the calamine that particle diameter is 80nm, add relative calamine weight and be 0.5% dispersant dialkyl dimethyl ammonium chloride and relative calamine in calamine weight Calamine weight is 1.5% dispersant sodium tripolyphosphate, then add deionized water to configure calamine slurry with a concentration of 22% by weight, put the calamine slurry in a ball mill, and ball mill for 120min to make Uniform nano calamine slurry;
[0040] (2) Spinning stock solution preparation process: the wood pulp with a degree of polymerization of about 800 and the cotton pulp with a degree of polymerization of 700 are mixed and pulverized at a weight ratio of 1:3, and then mixed with 1-butyl, 3-methylclomidazolium salt solution Mix evenly, dissolve at 110°C to form a uniform and stable spinning stock solution, and the concentration of ce...
Embodiment 3
[0047] Embodiment 3: the preparation method of calamine cellulose fiber, comprises the following steps:
[0048] (1) calamine slurry preparation process: get the calamine that particle diameter is 160nm, add relative calamine weight to be 0.6% dispersant polyalkyl trimethyl ammonium chloride and relative calamine in calamine weight Calamine weight is 0.9% dispersant sodium tripolyphosphate, and then add deionized water to configure calamine slurry with a concentration of 26% by weight, put the calamine slurry in a ball mill, and ball mill for 100 minutes to prepare Uniform nano calamine slurry;
[0049] (2) Spinning dope preparation process: the wood pulp with a degree of polymerization of 1000 and the bamboo pulp with a degree of polymerization of 900 are mixed and pulverized in a weight ratio of 5:1, and then mixed with chlorinated 1-(2-hydroxyethyl)-3- The methylimidazole solution is uniformly mixed, dissolved at 80°C to form a uniform and stable spinning stock solution, a...
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