Complex lithium-base lubricating grease and production technique thereof

A lithium-composite, lubricating grease technology, applied in lubricating compositions, petroleum industry, etc., can solve problems such as unsatisfactory anti-corrosion performance, reduced service life of bearings, and increased loss

Active Publication Date: 2011-05-11
辽宁海华科技股份有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0006] In wet and watery places, especially in seawater, its anti-rust performance is not ideal
[0007] In the case of a large amount of water flushing, the loss will increase, which is not good for bearing lubrication and sealing
[0008] In the case of heavy water load, the extreme pressure performance will be greatly reduced, the wear will be accelerated, and the service life of the bearing will be reduced

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0047] Lithium complex grease is characterized in that the proportioning by weight of each component is as follows:

[0048] 12 hydroxystearic acid: 9

[0049] Sebacic acid: 3

[0050] Lithium hydroxide: 2.6

[0051] Complex calcium sulfonate grease: 5

[0052] Base oil: 78.3

[0053] Tackifier: 0.5

[0054] Multifunctional agent: 1

[0055] Antioxidant: 0.5

[0056] Metal deactivator: 0.1

[0057] The production process of the complex lithium-based grease is as follows: add the prefabricated A product into the B product, disperse evenly through stirring and circular shearing, and obtain the finished product.

[0058] A product manufacturing method: convert super high base value calcium sulfonate and conversion agent at 60-100°C for 20-60 minutes, until it thickens obviously, heat to 140-180°C to remove water, and set aside; the conversion agent accounts for calcium sulfonate 4-10% by weight. The conversion agent is a mixture of low-carbon alcohol, organic acid and wate...

Embodiment 2

[0061] Lithium complex grease is characterized in that the proportioning by weight of each component is as follows:

[0062] 12 hydroxystearic acid: 11.2

[0063] Sebacic acid: 3.8

[0064] Lithium hydroxide: 3.2

[0065] Complex calcium sulfonate grease: 30

[0066] Base oil: 47.3

[0067] Tackifier: 0.8

[0068] Multifunctional agent: 2.7

[0069] Antioxidant: 0.8

[0070] Metal deactivator: 0.2

[0071] The production technology of complex lithium base lubricating grease is the same as embodiment 1.

Embodiment 3

[0073] Lithium complex grease is characterized in that the proportioning by weight of each component is as follows:

[0074] 12 hydroxystearic acid: 13.5

[0075] Sebacic acid: 4.5

[0076] Lithium hydroxide: 3.9

[0077] Complex calcium sulfonate grease: 50

[0078] Base oil: 22.8

[0079] Tackifier: 1

[0080] Multipurpose agent: 3

[0081] Antioxidant: 1

[0082] Metal deactivator: 0.3

[0083] The production technology of complex lithium base lubricating grease is the same as embodiment 1.

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Abstract

The invention relates to a complex lithium-base lubricating grease and a production technique thereof. The complex lithium-base lubricating grease comprises the following components in parts by weight: 9-13.5 parts of 12 hydroxystearic acid, 3-4.5 parts of decanedioic acid, 2.6-3.9 parts of lithium hydroxide, 5-50 parts of compound calcium sulfonate lubricating grease, 22.8-78.3 parts of base oil, 0.5-1 part of thickener, 1-3 parts of multifunctional agent, 0.5-1 part of antioxidant and 0.1-0.3 part of metal deactivator. The production technique comprises the following steps: converting superhigh-base-number calcium sulfonate with a conversion agent at 60-100 DEG C for 20-60 minutes until the superhigh-base-number calcium sulfonate becomes obviously thickened, and heating to 140-180 DEG Cto remove water, thereby obtaining the complex calcium sulfonate lubricating grease. The invention has the advantages of long service life in the occasions of long grease-complementation period under long-term heavy load, slight oxidative stain at high temperature, excellent anti-rusting property in damp or sea occasions, and low loss in the occasions of substantive water flushing; and the invention has favorable lubricating property and can prolong the service life of the bearing in the occasions of dampness and heavy load.

Description

technical field [0001] The invention relates to a lubricating grease and a production process thereof. Background technique [0002] Lithium complex grease is a high-quality high-temperature grease widely used in the lubrication of equipment bearings in mining, metallurgy, steel rolling, automobile, chemical industry, machinery, ships and other fields. Its advantages are high dropping point and wide applicable temperature range; colloidal stability and shear resistance are better than ordinary lithium-based grease, and its service life is longer than ordinary lithium-based grease; the leakage is small, it is not easy to lose in the bearing, and it saves lubrication The amount of fat used. [0003] However, there are also deficiencies in the use under some harsh conditions, as shown in the following aspects: [0004] In the case of long-term operation and long grease filling cycle, the bearing life of complex lithium-based grease cannot fully meet the requirements, especial...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C10M169/06C10N30/12C10N50/10C10N40/02
Inventor 刘鹏王庆日赵丽张晓芳石峰杨家栋王亮吕焕明李元鸿田微邹存斗杜尚君李明慧
Owner 辽宁海华科技股份有限公司
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