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Lead-free low-melting-point glass powder and production process thereof

A low-melting point glass and process technology, applied in the field of inorganic materials, can solve problems such as poor performance, physical injury of production workers, environmental pollution, etc., and achieve the effect of low softening temperature and working temperature, and better softening temperature and working temperature

Inactive Publication Date: 2013-01-16
浙江鼎昇新材料科技股份有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] The original low-melting point glass often contained harmful metals such as lead, which was likely to cause environmental pollution and physical injury to production workers. Although the later low-melting point glass improved this defect, it still performed poorly in low-temperature softening and low-temperature work. Requires higher temperatures to soften and flow for soldering

Method used

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Embodiment Construction

[0013] The present invention will be further described below in conjunction with embodiment:

[0014] The formula of the lead-free low-melting glass powder of the present invention is composed of component A and component B, wherein the mass ratio of each raw material in component A is: SiO2: 2-28, CaO: 27-40, ZnO: 2~7, B2O3: 1~11, Na20: 1~4, K2O: 1~3, F-: 1~2, MgO: 0.1~3, Sb2O3: 1~2, MoO3: 0.5~5, WO3 : 0.5 ~ 5, Li2O: 1 ~ 5; B component is thermal expansion regulating powder, the mass ratio of B component and A component is 1:4 ~ 2:3, thermal expansion regulating powder is nepheline or pyroxene.

[0015] The production technique of lead-free low-melting point glass powder of the present invention comprises steps as follows:

[0016] (1) Prepare component A according to the above mass ratio, and use a crucible to heat it at 1100-1300°C to melt it into molten glass;

[0017] (2) Pour the molten glass into the prepared mold for shaping, water quenching, and breaking the glass b...

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PUM

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Abstract

The invention relates to lead-free low-melting point glass powder and a production process thereof. A formula of the lead-free low-melting-point glass powder comprises a component A and a component B, wherein the component A comprises the following raw materials by mass ratio: SiO2 2-28, CaO 27-40, ZnO 2-7, B2O3 1-11, Na2O 1-4, K2O 1-3, F<-> 1-2, MgO 0.1-3, Sb2O3 1-2, MoO3 0.5-5, WO3 0.5-5 and Li2O 1-5; the component B is thermal expansion regulating powder; and the mass ratio of the component B to the component A is 1:4-2:3. The invention has the advantages of improving the formula on the basis of a production technology of the traditional low-melting-point glass and then forming into powder through melting, water quenching and ball-milling processes, thereby meeting the requirements on lead-free environmental protection and lower softening temperature and working temperature.

Description

technical field [0001] The invention belongs to the field of inorganic materials, in particular to a lead-free low-melting glass powder and a production process. Background technique [0002] Low-melting point glass can be used as a welding material for glass. It is widely used in the sealing and bonding of electronic devices such as electro-optical tubes and electron tubes, as well as components such as semiconductors. It can also be used in the connection between glass materials and the repair of surface defects. , from the beginning of its appearance, there have been many varieties with large differences in performance. [0003] The original low-melting point glass often contained harmful metals such as lead, which was likely to cause environmental pollution and physical injury to production workers. Although the later low-melting point glass improved this defect, it still performed poorly in low-temperature softening and low-temperature work. Higher temperatures are req...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C03C12/00
Inventor 赵金山高尔明
Owner 浙江鼎昇新材料科技股份有限公司